(3S,4R)-3-Amino-1-[(R)-[1,3]dithian-2-yl-((4S,5R,4'R)-2,2,2',2'-tetramethyl-[4,4']bi[[1,3]dioxolanyl]-5-yl)-methyl]-4-((E)-styryl)-azetidin-2-one

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Chemical Name:(3S,4R)-3-Amino-1-[(R)-[1,3]dithian-2-yl-((4S,5R,4'R)-2,2,2',2'-tetramethyl-[4,4']bi[[1,3]dioxolanyl]-5-yl)-methyl]-4-((E)-styryl)-azetidin-2-one
CAS No.:131991-02-1
Molecular Formula:C₂₆H₃₆N₂O₅S₂
Molecular Weight:520.714
Hs Code.:

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Chemical Property of (3S,4R)-3-Amino-1-[(R)-[1,3]dithian-2-yl-((4S,5R,4'R)-2,2,2',2'-tetramethyl-[4,4']bi[[1,3]dioxolanyl]-5-yl)-methyl]-4-((E)-styryl)-azetidin-2-one

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Technology Process of (3S,4R)-3-Amino-1-[(R)-[1,3]dithian-2-yl-((4S,5R,4'R)-2,2,2',2'-tetramethyl-[4,4']bi[[1,3]dioxolanyl]-5-yl)-methyl]-4-((E)-styryl)-azetidin-2-one

There total 4 articles about (3S,4R)-3-Amino-1-[(R)-[1,3]dithian-2-yl-((4S,5R,4'R)-2,2,2',2'-tetramethyl-[4,4']bi[[1,3]dioxolanyl]-5-yl)-methyl]-4-((E)-styryl)-azetidin-2-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 131991-00-9
2-[(3S,4R)-1-[(R)-[1,3]Dithian-2-yl-((4S,5R,4'R)-2,2,2',2'-tetramethyl-[4,4']bi[[1,3]dioxolanyl]-5-yl)-methyl]-2-oxo-4-((E)-styryl)-azetidin-3-yl]-isoindole-1,3-dione

: 131991-02-1
(3S,4R)-3-Amino-1-[(R)-[1,3]dithian-2-yl-((4S,5R,4'R)-2,2,2',2'-tetramethyl-[4,4']bi[[1,3]dioxolanyl]-5-yl)-methyl]-4-((E)-styryl)-azetidin-2-one

Guidance literature:: With methylhydrazine; In dichloromethane;

Reference yield:

: 3416-24-8
2-amino-2-deoxyglucose

: 131991-02-1
(3S,4R)-3-Amino-1-[(R)-[1,3]dithian-2-yl-((4S,5R,4'R)-2,2,2',2'-tetramethyl-[4,4']bi[[1,3]dioxolanyl]-5-yl)-methyl]-4-((E)-styryl)-azetidin-2-one

Guidance literature:: Multi-step reaction with 5 steps

1: 92 percent / conc. hydrochloric acid / 1.) 0 degC, 2 h, 2.) 60 degC, 12 h

2: 90 percent / p-TSOH/H₂SO₄ / dimethylformamide

4: 92 percent / triethylamine / 0.08 h

5: methylhydrazine / CH₂Cl₂

With hydrogenchloride; sulfuric acid; toluene-4-sulfonic acid; triethylamine; methylhydrazine; In dichloromethane; N,N-dimethyl-formamide;

Reference yield:

: 72022-71-0
2-amino-2-deoxy-D-glucose propane-1,3-diyldithioacetal hydrochloride

: 131991-02-1
(3S,4R)-3-Amino-1-[(R)-[1,3]dithian-2-yl-((4S,5R,4'R)-2,2,2',2'-tetramethyl-[4,4']bi[[1,3]dioxolanyl]-5-yl)-methyl]-4-((E)-styryl)-azetidin-2-one

Guidance literature:: Multi-step reaction with 4 steps

1: 90 percent / p-TSOH/H₂SO₄ / dimethylformamide

3: 92 percent / triethylamine / 0.08 h

4: methylhydrazine / CH₂Cl₂

With sulfuric acid; toluene-4-sulfonic acid; triethylamine; methylhydrazine; In dichloromethane; N,N-dimethyl-formamide;