Technology Process of 17β-Hydroxy-4aα-methyl-A-homo-B,19-dinor-5β,10α-androstan-3-one 17-Cyclohexanecarboxylate
There total 6 articles about 17β-Hydroxy-4aα-methyl-A-homo-B,19-dinor-5β,10α-androstan-3-one 17-Cyclohexanecarboxylate which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
Multi-step reaction with 6 steps
1: 93 percent / Lithium terc-butoxyaluminium hydride / tetrahydrofuran / 1 h / Ambient temperature
2: 78 percent / Pyridine / 2 h / Ambient temperature
3: 44 percent / Silver Acetate / acetic acid / 20 h / Heating
4: 42 percent / Hydrogen / Platinum oxide / acetic acid / 6 h / Ambient temperature
5: 86 percent / Methanol, Hydrochloric Acid / CHCl3 / 48 h / Ambient temperature
6: 765 mg / Jones reagent / acetone / 0.08 h / Ambient temperature
With
pyridine; hydrogenchloride; methanol; jones reagent; lithium tert-butoxyaluminium hydride; hydrogen; silver(I) acetate;
platinum(IV) oxide;
In
tetrahydrofuran; chloroform; acetic acid; acetone;
- Guidance literature:
-
Multi-step reaction with 3 steps
1: 42 percent / Hydrogen / Platinum oxide / acetic acid / 6 h / Ambient temperature
2: 86 percent / Methanol, Hydrochloric Acid / CHCl3 / 48 h / Ambient temperature
3: 765 mg / Jones reagent / acetone / 0.08 h / Ambient temperature
With
hydrogenchloride; methanol; jones reagent; hydrogen;
platinum(IV) oxide;
In
chloroform; acetic acid; acetone;
- Guidance literature:
-
Multi-step reaction with 5 steps
1: 78 percent / Pyridine / 2 h / Ambient temperature
2: 44 percent / Silver Acetate / acetic acid / 20 h / Heating
3: 42 percent / Hydrogen / Platinum oxide / acetic acid / 6 h / Ambient temperature
4: 86 percent / Methanol, Hydrochloric Acid / CHCl3 / 48 h / Ambient temperature
5: 765 mg / Jones reagent / acetone / 0.08 h / Ambient temperature
With
pyridine; hydrogenchloride; methanol; jones reagent; hydrogen; silver(I) acetate;
platinum(IV) oxide;
In
chloroform; acetic acid; acetone;
