4aα-Methyl-A-homo-5,19-dinor-5β,10α-androstane-3β,17β-diol 17-Cyclohexanecarboxylate

Base Information

Chemical Name:4aα-Methyl-A-homo-5,19-dinor-5β,10α-androstane-3β,17β-diol 17-Cyclohexanecarboxylate
CAS No.:126821-01-0
Molecular Formula:C₂₆H₄₂O₃
Molecular Weight:402.618
Hs Code.:

Synonyms:4aα-Methyl-A-homo-5,19-dinor-5β,10α-androstane-3β,17β-diol 17-Cyclohexanecarboxylate

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Chemical Property of 4aα-Methyl-A-homo-5,19-dinor-5β,10α-androstane-3β,17β-diol 17-Cyclohexanecarboxylate

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Technology Process of 4aα-Methyl-A-homo-5,19-dinor-5β,10α-androstane-3β,17β-diol 17-Cyclohexanecarboxylate

There total 5 articles about 4aα-Methyl-A-homo-5,19-dinor-5β,10α-androstane-3β,17β-diol 17-Cyclohexanecarboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

: 126792-31-2
4aα-Methyl-A-homo-B,19-dinor-5β,10α-androstane-3β,17β-diol 3-Acetate 17-Cyclohexanecarboxylate

: 126821-01-0
4aα-Methyl-A-homo-5,19-dinor-5β,10α-androstane-3β,17β-diol 17-Cyclohexanecarboxylate

Guidance literature:: With hydrogenchloride; methanol; In chloroform; for 48h; Ambient temperature;

Reference yield:

: 6961-53-1
3β-Acetoxy-6β-chloro-5-methyl-19-nor-5β-androst-9-en-17-one

: 126821-01-0
4aα-Methyl-A-homo-5,19-dinor-5β,10α-androstane-3β,17β-diol 17-Cyclohexanecarboxylate

Guidance literature:: Multi-step reaction with 5 steps

1: 93 percent / Lithium terc-butoxyaluminium hydride / tetrahydrofuran / 1 h / Ambient temperature

2: 78 percent / Pyridine / 2 h / Ambient temperature

3: 44 percent / Silver Acetate / acetic acid / 20 h / Heating

4: 42 percent / Hydrogen / Platinum oxide / acetic acid / 6 h / Ambient temperature

5: 86 percent / Methanol, Hydrochloric Acid / CHCl₃ / 48 h / Ambient temperature

With pyridine; hydrogenchloride; methanol; lithium tert-butoxyaluminium hydride; hydrogen; silver(I) acetate; platinum(IV) oxide; In tetrahydrofuran; chloroform; acetic acid;

Reference yield:

: 126792-29-8
4a-Methyleno-A-homo-B,19-dinor-5β-androst-9-ene-3β,17β-diol 3-Acetate 17-Benzoate

: 126821-01-0
4aα-Methyl-A-homo-5,19-dinor-5β,10α-androstane-3β,17β-diol 17-Cyclohexanecarboxylate

Guidance literature:: Multi-step reaction with 2 steps

1: 42 percent / Hydrogen / Platinum oxide / acetic acid / 6 h / Ambient temperature

2: 86 percent / Methanol, Hydrochloric Acid / CHCl₃ / 48 h / Ambient temperature

With hydrogenchloride; methanol; hydrogen; platinum(IV) oxide; In chloroform; acetic acid;