N,N'-Bis--thiocarbanilid

Base Information

• Chemical Name: N,N'-Bis--thiocarbanilid
• CAS No.: 22136-24-9
• Molecular Formula: C₂₃H₃₂N₂O₄S
• Molecular Weight: 432.584
• Mol file: 22136-24-9.mol

Synonyms:

Chemical Property of N,N'-Bis--thiocarbanilid

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of N,N'-Bis--thiocarbanilid

There total 4 articles about N,N'-Bis--thiocarbanilid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

1-(isopentyloxy)-4-nitrobenzene (7244-79-3) → N,N'-Bis--thiocarbanilid (22136-24-9)

Guidance literature:

Multi-step reaction with 4 steps

1: CrO₃ / acetic acid

2: H₂ / Pd-C

3: aq. HCl

4: propan-2-ol / Heating

With chromium(VI) oxide; hydrogenchloride; hydrogen; palladium on activated charcoal; In acetic acid; isopropyl alcohol;

DOI:10.1002/hlca.19690520515

Reference yield:

3-methyl-1-(4-nitrophenoxy)butan-3-ol (10572-18-6) → N,N'-Bis--thiocarbanilid (22136-24-9)

Guidance literature:

Multi-step reaction with 3 steps

1: H₂ / Pd-C

2: aq. HCl

3: propan-2-ol / Heating

With hydrogenchloride; hydrogen; palladium on activated charcoal; In isopropyl alcohol;

DOI:10.1002/hlca.19690520515

Reference yield:

1-(4-aminophenoxy)-3-methylbutan-3-ol → N,N'-Bis--thiocarbanilid (22136-24-9)

Guidance literature:

Multi-step reaction with 2 steps

1: aq. HCl

2: propan-2-ol / Heating

With hydrogenchloride; In isopropyl alcohol;

DOI:10.1002/hlca.19690520515

upstream raw materials:

1-(isopentyloxy)-4-nitrobenzene

3-methyl-1-(4-nitrophenoxy)butan-3-ol

Downstream raw materials:

N--N'--thiocarbanilid