(((C₆H₁₁)2P)2CH₂)Rh(OC(CF₃))2CH

Base Information

• Chemical Name: (((C₆H₁₁)2P)2CH₂)Rh(OC(CF₃))2CH
• CAS No.: 222017-64-3
• Molecular Formula: C₃₀H₄₇F₆O₂P₂Rh
• Molecular Weight: 718.545
• Mol file: 222017-64-3.mol

Synonyms:

Chemical Property of (((C₆H₁₁)2P)2CH₂)Rh(OC(CF₃))2CH

Chemical Property:

Purity/Quality:

Safty Information:

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Useful:

Technology Process of (((C₆H₁₁)2P)2CH₂)Rh(OC(CF₃))2CH

There total 1 articles about (((C₆H₁₁)2P)2CH₂)Rh(OC(CF₃))2CH which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

(hexafluoroacetylacetonato)(1,5-cyclooctadiene)rhodium(I) + bis(dicyclohexylphosphino)methane (137349-65-6) → (((C6H11)2P)2CH2)Rh(OC(CF3))2CH (222017-64-3) + ((((C6H11)2P)2CH2)Rh)2((OC(CF3))2CH)2

Guidance literature:

In tetrahydrofuran; Ar-atmosphere; slow phosphine soln. addn.; crystn.; elem. anal.;

DOI:10.1021/om980980k

Reference yield: 8.0%

(((C6H11)2P)2CH2)Rh(OC(CF3))2CH (222017-64-3) → [(OC(CF3))2CHRh(((C6H11)2P)2CH2)2Rh(OC(CF3))2CH]

Guidance literature:

In benzene-d6; standing (78 h);

DOI:10.1021/om980980k

upstream raw materials:

bis(dicyclohexylphosphino)methane