[1,2,4]Triazolo[4,3-a]quinoxaline-1,4(2H,5H)-dione,7-chloro-2-(1-oxo-3-phenyl-2-propen-1-yl)-5-propyl-

Base Information

Chemical Name:[1,2,4]Triazolo[4,3-a]quinoxaline-1,4(2H,5H)-dione,7-chloro-2-(1-oxo-3-phenyl-2-propen-1-yl)-5-propyl-
CAS No.:90042-36-7
Molecular Formula:C₂₁H₁₇ClN₄O₃
Molecular Weight:408.844
Hs Code.:

Synonyms:[1,2,4]Triazolo[4,3-a]quinoxaline-1,4(2H,5H)-dione,7-chloro-2-(1-oxo-3-phenyl-2-propenyl)-5-propyl- (9CI); REV 3899; RHC 3899

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Chemical Property of [1,2,4]Triazolo[4,3-a]quinoxaline-1,4(2H,5H)-dione,7-chloro-2-(1-oxo-3-phenyl-2-propen-1-yl)-5-propyl-

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MSDS Files:: SDS file from LookChem

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Technology Process of [1,2,4]Triazolo[4,3-a]quinoxaline-1,4(2H,5H)-dione,7-chloro-2-(1-oxo-3-phenyl-2-propen-1-yl)-5-propyl-

There total 5 articles about [1,2,4]Triazolo[4,3-a]quinoxaline-1,4(2H,5H)-dione,7-chloro-2-(1-oxo-3-phenyl-2-propen-1-yl)-5-propyl- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 66315-16-0
methyl 3-amino-4-(methylamino)benzoate

: 90042-36-7
7-Chloro-2-[(E)-(3-phenyl-acryloyl)]-5-propyl-2H,5H-[1,2,4]triazolo[4,3-a]quinoxaline-1,4-dione

Guidance literature:: Multi-step reaction with 5 steps

1: various solvent(s) / 1 h / 130 °C

2: SOCl₂ / toluene; dimethylformamide / 2 h / 130 °C

3: acetonitrile / 2 h / 120 °C

4: various solvent(s) / 0.42 h / 220 - 230 °C

5: pyridine / 3 h / 100 °C

With pyridine; thionyl chloride; In N,N-dimethyl-formamide; toluene; acetonitrile;
DOI:10.1021/jm00381a016

Reference yield:

: 92473-55-7
methyl 1-methyl-2,3-dioxo-1,2,3,4-tetrahydroquinoxaline-6-carboxylate

: 90042-36-7
7-Chloro-2-[(E)-(3-phenyl-acryloyl)]-5-propyl-2H,5H-[1,2,4]triazolo[4,3-a]quinoxaline-1,4-dione

Guidance literature:: Multi-step reaction with 4 steps

1: SOCl₂ / toluene; dimethylformamide / 2 h / 130 °C

2: acetonitrile / 2 h / 120 °C

3: various solvent(s) / 0.42 h / 220 - 230 °C

4: pyridine / 3 h / 100 °C

With pyridine; thionyl chloride; In N,N-dimethyl-formamide; toluene; acetonitrile;
DOI:10.1021/jm00381a016

Reference yield:

: 1246738-34-0
3-Chloro-1-methyl-2-oxo-1,2-dihydro-quinoxaline-6-carboxylic acid methyl ester

: 90042-36-7
7-Chloro-2-[(E)-(3-phenyl-acryloyl)]-5-propyl-2H,5H-[1,2,4]triazolo[4,3-a]quinoxaline-1,4-dione

Guidance literature:: Multi-step reaction with 3 steps

1: acetonitrile / 2 h / 120 °C

2: various solvent(s) / 0.42 h / 220 - 230 °C

3: pyridine / 3 h / 100 °C

With pyridine; In acetonitrile;
DOI:10.1021/jm00381a016