S-phenyl tetrafluoro-2-(phenylthio)propanethioate

Base Information

• Chemical Name: S-phenyl tetrafluoro-2-(phenylthio)propanethioate
• CAS No.: 227954-75-8
• Molecular Formula: C₁₅H₁₀F₄OS₂
• Molecular Weight: 346.369

Synonyms:

Chemical Property of S-phenyl tetrafluoro-2-(phenylthio)propanethioate

Chemical Property:

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Technology Process of S-phenyl tetrafluoro-2-(phenylthio)propanethioate

There total 1 articles about S-phenyl tetrafluoro-2-(phenylthio)propanethioate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 74.0%

Hexafluoropropene oxide (428-59-1,25038-02-2) + thiophenol (108-98-5) → S-phenyl pentafluoropropanethioate + S-phenyl tetrafluoro-2-(phenylthio)propanethioate (227954-75-8)

Guidance literature:

With potassium hydroxide; Yield given; 1.) MeOH, r.t., 24 h, 2.) THF, r.t., 15 h;

Reference yield: 42.0%

S-phenyl tetrafluoro-2-(phenylthio)propanethioate (227954-75-8) → (R,S)-1,2,2,2-tetrafluoro-1-(phenylthio)ethane (130612-76-9)

Guidance literature:

With water; silver nitrate; In 1,4-dioxane; for 4h; Heating;

Reference yield:

S-phenyl tetrafluoro-2-(phenylthio)propanethioate (227954-75-8) → 2,3,3,3-tetrafluoro-2-(phenylthio)propanoic acid

Guidance literature:

With potassium hydroxide; water; for 18h; Yield given; Heating;

upstream raw materials:

Hexafluoropropene oxide

thiophenol

Downstream raw materials:

(R,S)-1,2,2,2-tetrafluoro-1-(phenylthio)ethane

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