Technology Process of C32H36N6O6
There total 5 articles about C32H36N6O6 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
Multi-step reaction with 3 steps
1: sodium azide / N,N-dimethyl-formamide / 12 h / 70 °C
2: hydrazine / ethanol; water / 12 h / 80 °C
3: copper(II) sulfate; sodium L-ascorbate / pH 7.5 / aq. phosphate buffer
With
sodium azide; copper(II) sulfate; sodium L-ascorbate; hydrazine;
In
ethanol; water; N,N-dimethyl-formamide;
DOI:10.1002/anie.201101331
- Guidance literature:
-
Multi-step reaction with 2 steps
1: hydrazine / ethanol; water / 12 h / 80 °C
2: copper(II) sulfate; sodium L-ascorbate / pH 7.5 / aq. phosphate buffer
With
copper(II) sulfate; sodium L-ascorbate; hydrazine;
In
ethanol; water;
DOI:10.1002/anie.201101331
- Guidance literature:
-
Multi-step reaction with 5 steps
1: sodium tetrahydroborate / ethanol / 20 °C / Cooling with ice
2: phosphorus tribromide / dichloromethane / 20 °C / Inert atmosphere; Cooling with ice
3: sodium azide / N,N-dimethyl-formamide / 12 h / 70 °C
4: hydrazine / ethanol; water / 12 h / 80 °C
5: copper(II) sulfate; sodium L-ascorbate / pH 7.5 / aq. phosphate buffer
With
sodium tetrahydroborate; sodium azide; phosphorus tribromide; copper(II) sulfate; sodium L-ascorbate; hydrazine;
In
ethanol; dichloromethane; water; N,N-dimethyl-formamide;
DOI:10.1002/anie.201101331