C₂₃H₂₆O₅

Base Information

Chemical Name:C₂₃H₂₆O₅
CAS No.:1426547-63-8
Molecular Formula:C₂₃H₂₆O₅
Molecular Weight:382.456
Hs Code.:

C<sub>23</sub>H<sub>26</sub>O<sub>5</sub>

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₂₃H₂₆O₅

Chemical Property:

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Technology Process of C₂₃H₂₆O₅

There total 12 articles about C₂₃H₂₆O₅ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1426547-62-7
C₂₂H₂₄O₅

: 74-88-4
methyl iodide

: 1426547-63-8
C₂₃H₂₆O₅

Guidance literature:: With sodium hydride; In N,N-dimethyl-formamide; mineral oil; at 0 - 20 ℃; for 6h; Inert atmosphere;
DOI:10.1021/ja311902f

Reference yield:

: 1076-26-2
1-methyl-2-naphthol

: 1426547-63-8
C₂₃H₂₆O₅

Guidance literature:: Multi-step reaction with 7 steps

1.1: sodium hydride / N,N-dimethyl-formamide; mineral oil / 8 h / 0 - 20 °C / Inert atmosphere

2.1: n-butyllithium / hexane; diethyl ether / 3 h / 0 - 20 °C / Inert atmosphere

2.2: 0.17 h / 0 °C / Inert atmosphere

3.1: montmorillonite K-10 / benzene / 1 h / 20 °C

4.1: potassium carbonate / acetone / 4.5 h / 0 - 20 °C

5.1: tetrakis(triphenylphosphine) palladium⁽⁰⁾; potassium phosphate / water; 1,2-dimethoxyethane / 3.5 h / Reflux

6.1: lithium aluminium tetrahydride / tetrahydrofuran / 0.5 h / 0 °C / Inert atmosphere

6.2: 1 h / 20 °C / Inert atmosphere

7.1: sodium hydride / N,N-dimethyl-formamide; mineral oil / 6 h / 0 - 20 °C / Inert atmosphere

With potassium phosphate; lithium aluminium tetrahydride; tetrakis(triphenylphosphine) palladium⁽⁰⁾; n-butyllithium; sodium hydride; potassium carbonate; In tetrahydrofuran; 1,2-dimethoxyethane; diethyl ether; hexane; water; N,N-dimethyl-formamide; acetone; mineral oil; benzene; 5.1: |Suzuki Coupling;
DOI:10.1021/ja311902f

Reference yield:

: 1426547-58-1
3-(methoxymethoxy)-4-methyl-2-naphthaldehyde

: 1426547-63-8
C₂₃H₂₆O₅

Guidance literature:: Multi-step reaction with 5 steps

1.1: montmorillonite K-10 / benzene / 1 h / 20 °C

2.1: potassium carbonate / acetone / 4.5 h / 0 - 20 °C

3.1: tetrakis(triphenylphosphine) palladium⁽⁰⁾; potassium phosphate / water; 1,2-dimethoxyethane / 3.5 h / Reflux

4.1: lithium aluminium tetrahydride / tetrahydrofuran / 0.5 h / 0 °C / Inert atmosphere

4.2: 1 h / 20 °C / Inert atmosphere

5.1: sodium hydride / N,N-dimethyl-formamide; mineral oil / 6 h / 0 - 20 °C / Inert atmosphere

With potassium phosphate; lithium aluminium tetrahydride; tetrakis(triphenylphosphine) palladium⁽⁰⁾; sodium hydride; potassium carbonate; In tetrahydrofuran; 1,2-dimethoxyethane; water; N,N-dimethyl-formamide; acetone; mineral oil; benzene; 3.1: |Suzuki Coupling;
DOI:10.1021/ja311902f