[(μ-2,6-(i-Pr)2C6H3NC(Ph)CH2CH2NMe2)FeCl]2

Base Information

Chemical Name:[(μ-2,6-(i-Pr)2C6H3NC(Ph)CH2CH2NMe2)FeCl]2
CAS No.:1024803-55-1
Molecular Formula:C₄₆H₆₄Cl₂Fe₂N₆
Molecular Weight:883.654
Hs Code.:

Synonyms:

Suppliers and Price of [(μ-2,6-(i-Pr)2C6H3NC(Ph)CH2CH2NMe2)FeCl]2

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of [(μ-2,6-(i-Pr)2C6H3NC(Ph)CH2CH2NMe2)FeCl]2

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of [(μ-2,6-(i-Pr)2C6H3NC(Ph)CH2CH2NMe2)FeCl]2

There total 1 articles about [(μ-2,6-(i-Pr)2C6H3NC(Ph)CH2CH2NMe2)FeCl]2 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 40.0%

: Li(2,6-(i-Pr)2C₆H₃NC(Ph)CH₂CH₂NMe₂)

: iron(II) chloride

: 1024803-55-1
[(μ-2,6-(i-Pr)2C6H3NC(Ph)CH2CH2NMe2)FeCl]2

Guidance literature:: In tetrahydrofuran; (N2); std. Schlenk technique; soln. of Li salt (1 equiv.) and FeCl2 (1 equiv.) in THF was stirred for 20 min; solvent removed (vac.); stirred with pentane; pumped; washed (pentane); extd. (toluene); concd.; warmed to 80°C; cooled to room temp.; elem. anal.;
DOI:10.1021/om701155b

Reference yield: 81.0%

: 1024803-55-1
[(μ-2,6-(i-Pr)2C6H3NC(Ph)CH2CH2NMe2)FeCl]2

: 201230-82-2
carbon monoxide

: [(κ3-C(O)(2,6-(i-Pr)2C6H3)NC(Ph)CH2CH2NMe2)FeCl(CO)2]

Guidance literature:: In toluene; (N2); std. Schlenk technique; soln. of Fe complex in toluene was degassed; CO (1 atm) was admitted; stirred at room temp. for 2 d; solvent removed (vac.); extd. (pentane); concd.; cooled to -80°C;elem. anal.;
DOI:10.1021/om701155b

Reference yield: 43.0%

: 1024803-55-1
[(μ-2,6-(i-Pr)2C6H3NC(Ph)CH2CH2NMe2)FeCl]2

: 2785-29-7
benzyl potassium

: [(μ-Me3SiNC(Ph)CH2CH2NMe2)Fe(benzyl)]2

Guidance literature:: In tetrahydrofuran; (N2); std. Schlenk technique; suspn. of Fe complex and KCH2Ph in THF wasallowed to warm from -40°C to room temp. while stirring; stirred at room temp. for 1 h; evapd. (vac.); stirred with pentane; pumped; extd. (Et2O); evapd.; recrystd. (toluene, 80-100°C); elem. anal.;
DOI:10.1021/om701155b