Technology Process of 2,3,4,6-tetra-O-benzoyl-α-D-idopyranose
There total 6 articles about 2,3,4,6-tetra-O-benzoyl-α-D-idopyranose which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
Multi-step reaction with 4 steps
1: boron trifluoride diethyl etherate / dichloromethane / 4 h / 20 °C / Molecular sieve
2: methanol; sodium methylate / 1 h
3: pyridine
4: hydrogen; palladium 10% on activated carbon / 16 h
With
pyridine; methanol; palladium 10% on activated carbon; boron trifluoride diethyl etherate; hydrogen; sodium methylate;
In
dichloromethane;
DOI:10.1002/ejoc.201402187
- Guidance literature:
-
Multi-step reaction with 4 steps
1: trimethylsilyl trifluoromethanesulfonate / dichloromethane / 0.33 h / 0 °C / Molecular sieve
2: methanol; sodium methylate / 1 h
3: pyridine
4: hydrogen; palladium 10% on activated carbon / 16 h
With
pyridine; methanol; trimethylsilyl trifluoromethanesulfonate; palladium 10% on activated carbon; hydrogen; sodium methylate;
In
dichloromethane;
DOI:10.1002/ejoc.201402187
- Guidance literature:
-
Multi-step reaction with 4 steps
1: trimethylsilyl trifluoromethanesulfonate / dichloromethane / 0.33 h / 0 °C / Molecular sieve
2: methanol; sodium methylate / 1 h
3: pyridine
4: hydrogen; palladium 10% on activated carbon / 16 h
With
pyridine; methanol; trimethylsilyl trifluoromethanesulfonate; palladium 10% on activated carbon; hydrogen; sodium methylate;
In
dichloromethane;
DOI:10.1002/ejoc.201402187
