(S)-1-((S)-2-Amino-3-benzyloxy-propyldisulfanylmethyl)-2-benzyloxy-ethylamine; compound with trifluoro-acetic acid

Base Information

Chemical Name:(S)-1-((S)-2-Amino-3-benzyloxy-propyldisulfanylmethyl)-2-benzyloxy-ethylamine; compound with trifluoro-acetic acid
CAS No.:139429-19-9
Molecular Formula:2C₂HF₃O₂*C₂₀H₂₈N₂O₂S₂
Molecular Weight:620.634
Hs Code.:

Synonyms:

Suppliers and Price of (S)-1-((S)-2-Amino-3-benzyloxy-propyldisulfanylmethyl)-2-benzyloxy-ethylamine; compound with trifluoro-acetic acid

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of (S)-1-((S)-2-Amino-3-benzyloxy-propyldisulfanylmethyl)-2-benzyloxy-ethylamine; compound with trifluoro-acetic acid

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of (S)-1-((S)-2-Amino-3-benzyloxy-propyldisulfanylmethyl)-2-benzyloxy-ethylamine; compound with trifluoro-acetic acid

There total 3 articles about (S)-1-((S)-2-Amino-3-benzyloxy-propyldisulfanylmethyl)-2-benzyloxy-ethylamine; compound with trifluoro-acetic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 79069-15-1
N-(tert-butyloxycarbonyl)-O-benzyl-L-serinol

: 139429-19-9
(S)-1-((S)-2-Amino-3-benzyloxy-propyldisulfanylmethyl)-2-benzyloxy-ethylamine; compound with trifluoro-acetic acid

Guidance literature:: Multi-step reaction with 4 steps

1: diisopropyl azodicarboxylate, triphenylphosphine / tetrahydrofuran / Ambient temperature

2: 1 M NaOH / ethanol / a) 0 deg C, 1 h, b) RT, 3 h

3: I₂ / ethanol

4: CH₂Cl₂ / a) 0 deg C, 30 min, b) RT, 2 h

With sodium hydroxide; di-isopropyl azodicarboxylate; iodine; triphenylphosphine; In tetrahydrofuran; ethanol; dichloromethane;
DOI:10.1021/jm00085a013

Reference yield:

: 137719-74-5
(S)-3-(benzyloxy)-2-<(tert-butoxycarbonyl)amino>propyl ethanethioate

: 139429-19-9
(S)-1-((S)-2-Amino-3-benzyloxy-propyldisulfanylmethyl)-2-benzyloxy-ethylamine; compound with trifluoro-acetic acid

Guidance literature:: Multi-step reaction with 3 steps

1: 1 M NaOH / ethanol / a) 0 deg C, 1 h, b) RT, 3 h

2: I₂ / ethanol

3: CH₂Cl₂ / a) 0 deg C, 30 min, b) RT, 2 h

With sodium hydroxide; iodine; In ethanol; dichloromethane;
DOI:10.1021/jm00085a013

Reference yield:

: ((S)-2-Benzyloxy-1-mercaptomethyl-ethyl)-carbamic acid tert-butyl ester

: 139429-19-9
(S)-1-((S)-2-Amino-3-benzyloxy-propyldisulfanylmethyl)-2-benzyloxy-ethylamine; compound with trifluoro-acetic acid

Guidance literature:: Multi-step reaction with 2 steps

1: I₂ / ethanol

2: CH₂Cl₂ / a) 0 deg C, 30 min, b) RT, 2 h

With iodine; In ethanol; dichloromethane;
DOI:10.1021/jm00085a013