[Re2Br3(μ-dppm)2(CO)(2,6-dimethylphenyl isocyanide)]O3SCF3

Base Information

Chemical Name:[Re2Br3(μ-dppm)2(CO)(2,6-dimethylphenyl isocyanide)]O3SCF3
CAS No.:170242-81-6
Molecular Formula:CF₃O₃S*C₆₀H₅₃Br₃NOP₄Re₂
Molecular Weight:1689.18
Hs Code.:

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Chemical Property of [Re2Br3(μ-dppm)2(CO)(2,6-dimethylphenyl isocyanide)]O3SCF3

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Technology Process of [Re2Br3(μ-dppm)2(CO)(2,6-dimethylphenyl isocyanide)]O3SCF3

There total 2 articles about [Re2Br3(μ-dppm)2(CO)(2,6-dimethylphenyl isocyanide)]O3SCF3 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

: Re2Br4(μ-dppm)2(CO)(CNC6H3(CH3)2)

: 73491-36-8
thallium(I) triflate

: 170242-81-6
[Re2Br3(μ-dppm)2(CO)(2,6-dimethylphenyl isocyanide)]O3SCF3

Guidance literature:: In dichloromethane; byproducts: TlBr; N2-atmosphere; stirring equimolar amts. (25°C, 6 h); filtration off of TlBr, concn., addn. of isopropyl ether, crystn. on slow evapn. (25°C, 6 h); elem. anal.;
DOI:10.1021/ic00127a019

Reference yield: 78.0%

: 102781-92-0
Re2(μ-Br)(μ-dppm)2Br3(CO)

: 119072-54-7,2769-71-3
2,6-dimethylphenyl isonitrile

: 73491-36-8
thallium(I) triflate

: 170242-81-6
[Re2Br3(μ-dppm)2(CO)(2,6-dimethylphenyl isocyanide)]O3SCF3

Guidance literature:: In dichloromethane; byproducts: TlBr; N2-atmosphere; stirring equimolar amts.;
DOI:10.1021/ic00127a019

Reference yield: 81.0%

: 170242-81-6
[Re2Br3(μ-dppm)2(CO)(2,6-dimethylphenyl isocyanide)]O3SCF3

: 201230-82-2
carbon monoxide

: 181175-39-3
[Re2Br3(μ-dppm)2(CO)2(2,6-dimethylphenyl isocyanide)]O3SCF3

Guidance literature:: In dichloromethane; absence of air and moisture; bubbling CO for 30 s, then stirring at 25°C for 24 h; vol. reduction, C6H6 addn., crystn. on slow evapn. at 25°C; elem.anal.;