N-[(4-Methylphenyl)methylene]cyclobutanamine

Base Information

Chemical Name:N-[(4-Methylphenyl)methylene]cyclobutanamine
CAS No.:154777-47-6
Molecular Formula:C₁₂H₁₅N
Molecular Weight:173.258
Hs Code.:
DSSTox Substance ID:DTXSID601259593

Synonyms:154777-47-6;N-[(4-Methylphenyl)methylene]cyclobutanamine;DTXSID601259593

Suppliers and Price of N-[(4-Methylphenyl)methylene]cyclobutanamine

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N-[(4-Methylphenyl)methylene]cyclobutanamine

Chemical Property:

XLogP3:2.7
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:1
Rotatable Bond Count:2
Exact Mass:173.120449483
Heavy Atom Count:13
Complexity:174

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:CC1=CC=C(C=C1)C=NC2CCC2

Technology Process of N-[(4-Methylphenyl)methylene]cyclobutanamine

There total 1 articles about N-[(4-Methylphenyl)methylene]cyclobutanamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 2516-34-9
cyclobutylamine

: 104-87-0
4-methyl-benzaldehyde

: 154777-47-6
N-(p-methylbenzylidene)cyclobutylamine

Guidance literature:: With toluene-4-sulfonic acid; In toluene; for 2h; Heating;
DOI:10.1016/S0040-4020(01)80837-1

Reference yield:

: 154777-47-6
N-(p-methylbenzylidene)cyclobutylamine

: 16183-21-4
N-(4-methylbenzyl)butan-1-amine

Guidance literature:: Multi-step reaction with 3 steps

1: NaBH₄ / methanol / 2 h / Heating

2: 44 percent / toluene / 1 h / Heating

3: 1.) Bu₃SnH, AIBN; 2.) NaBH₄ / 1.) cyclohexane, 2 h, reflux; 2.) DMF/cyclohexane, r.t.

With sodium tetrahydroborate; 2,2'-azobis(isobutyronitrile); tri-n-butyl-tin hydride; In methanol; toluene;
DOI:10.1016/S0040-4020(01)80837-1

Reference yield:

: 154777-47-6
N-(p-methylbenzylidene)cyclobutylamine

: 138710-09-5
N-(benzenesulfenyl)-N-(p-methylbenzyl)cyclobutylamine

Guidance literature:: Multi-step reaction with 2 steps

1: NaBH₄ / methanol / 2 h / Heating

2: 44 percent / toluene / 1 h / Heating

With sodium tetrahydroborate; In methanol; toluene;
DOI:10.1016/S0040-4020(01)80837-1