himanimide B

Base Information

Chemical Name:himanimide B
CAS No.:464194-68-1
Molecular Formula:C₂₂H₂₃NO₅
Molecular Weight:381.428
Hs Code.:

Synonyms:

Suppliers and Price of himanimide B

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of himanimide B

Chemical Property:

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Technology Process of himanimide B

There total 6 articles about himanimide B which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 464895-13-4
3-benzyl-4-[4-(3-methylbut-2-enoxy)phenyl]-1H-pyrrole-2,5-dione

: C₂₂H₂₃NO₅

: 464194-68-1
himanimide B

Guidance literature:: With potassium osmate(VI) dihydrate; methanesulfonamide; hydroquinidine-2,5-diphenyl-4,6-pyrimidinediyl diether; potassium carbonate; potassium hexacyanoferrate(III); In dichloromethane; water; tert-butyl alcohol; at 0 - 20 ℃; for 22h; optical yield given as %ee; Inert atmosphere;
DOI:10.1002/asia.201000384

Reference yield:

: 1256724-50-1
1-(3-methylbut-2-enyloxy)-4-(3-phenylprop-1ynyl)benzene

: C₂₂H₂₃NO₅

: 464194-68-1
himanimide B

Guidance literature:: Multi-step reaction with 3 steps

1: triiron dodecarbonyl; ammonia / tetrahydrofuran / 20 h / 120 °C / 15001.5 Torr / Inert atmosphere

2: manganese(IV) oxide / toluene / 72 h / 90 - 110 °C / Inert atmosphere

3: potassium osmate(VI) dihydrate; hydroquinidine-2,5-diphenyl-4,6-pyrimidinediyl diether; methanesulfonamide; potassium carbonate; potassium hexacyanoferrate(III) / dichloromethane; water; tert-butyl alcohol / 22 h / 0 - 20 °C / Inert atmosphere

With manganese(IV) oxide; potassium osmate(VI) dihydrate; triiron dodecarbonyl; methanesulfonamide; hydroquinidine-2,5-diphenyl-4,6-pyrimidinediyl diether; ammonia; potassium carbonate; potassium hexacyanoferrate(III); In tetrahydrofuran; dichloromethane; water; toluene; tert-butyl alcohol; 3: Sharpless dihydroxylation;
DOI:10.1002/asia.201000384

Reference yield:

: 3-benzyl-4-(4-(3-methylbut-2-enyloxy)phenyl)pyrrolidine-2,5-dione

: C₂₂H₂₃NO₅

: 464194-68-1
himanimide B

Guidance literature:: Multi-step reaction with 2 steps

1: manganese(IV) oxide / toluene / 72 h / 90 - 110 °C / Inert atmosphere

2: potassium osmate(VI) dihydrate; hydroquinidine-2,5-diphenyl-4,6-pyrimidinediyl diether; methanesulfonamide; potassium carbonate; potassium hexacyanoferrate(III) / dichloromethane; water; tert-butyl alcohol / 22 h / 0 - 20 °C / Inert atmosphere

With manganese(IV) oxide; potassium osmate(VI) dihydrate; methanesulfonamide; hydroquinidine-2,5-diphenyl-4,6-pyrimidinediyl diether; potassium carbonate; potassium hexacyanoferrate(III); In dichloromethane; water; toluene; tert-butyl alcohol; 2: Sharpless dihydroxylation;
DOI:10.1002/asia.201000384