C₈H₁₇NO

Base Information

• Chemical Name: C₈H₁₇NO
• CAS No.: 1508307-49-0
• Molecular Formula: C₈H₁₇NO
• Molecular Weight: 143.229
• Mol file: 1508307-49-0.mol

Synonyms:

Chemical Property of C₈H₁₇NO

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₈H₁₇NO

There total 2 articles about C₈H₁₇NO which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

tert-butyl ((1s,4s)-4-(2-hydroxyethyl)cyclohexyl)carbamate (1069120-19-9) → C8H17NO (1508307-49-0)

Guidance literature:

With trifluoroacetic acid; In dichloromethane; at 20 ℃; for 4h; Cooling with ice;

DOI:10.1021/jm401370h

Reference yield:

((1s,4s)-4-((tert-butoxycarbonyl)amino)cyclohexyl)acetic acid (327156-95-6) → C8H17NO (1508307-49-0)

Guidance literature:

Multi-step reaction with 2 steps

1: borane-THF / tetrahydrofuran / 4 h / 0 - 20 °C

2: trifluoroacetic acid / dichloromethane / 4 h / 20 °C / Cooling with ice

With borane-THF; trifluoroacetic acid; In tetrahydrofuran; dichloromethane;

DOI:10.1021/jm401370h

Reference yield:

C8H17NO (1508307-49-0) → 2-((1s,4s)-4-azidocyclohexyl)ethanol (1508307-50-3)

Guidance literature:

With imidazole-1-sulfonyl azide hydrochloride; copper(ll) sulfate pentahydrate; potassium carbonate; In methanol; at 20 ℃; Cooling with ice;

DOI:10.1021/jm401370h

upstream raw materials:

((1s,4s)-4-((tert-butoxycarbonyl)amino)cyclohexyl)acetic acid

tert-butyl ((1s,4s)-4-(2-hydroxyethyl)cyclohexyl)carbamate

Downstream raw materials:

2-((1s,4s)-4-azidocyclohexyl)ethanol

C₈H₁₃N₃O

(E)-ethyl 4-((1s,4s)-4-azidocyclohexyl)-2-methylbut-2-enoate

(E)-4-((1s,4s)-4-azidocyclohexyl)-2-methylbut-2-en-1-ol