N-(2,3-dimethylphenyl)-4-nitrobenzamide

Base Information

Chemical Name:N-(2,3-dimethylphenyl)-4-nitrobenzamide
CAS No.:35709-76-3
Molecular Formula:C₁₅H₁₄N₂O₃
Molecular Weight:270.288
Hs Code.:
European Community (EC) Number:666-262-9

Synonyms:N-(2,3-dimethylphenyl)-4-nitrobenzamide;35709-76-3;Cambridge id 5306457;Oprea1_860114;STK358280;AKOS001423449;4-NITROBENZO-2',3'-XYLIDIDE

Suppliers and Price of N-(2,3-dimethylphenyl)-4-nitrobenzamide

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

American Custom Chemicals Corporation
4-NITROBENZO-2',3'-XYLIDIDE 95.00%
5MG
$ 498.41

Total 2 raw suppliers

Chemical Property of N-(2,3-dimethylphenyl)-4-nitrobenzamide

Chemical Property:

XLogP3:2.8
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:3
Rotatable Bond Count:2
Exact Mass:270.10044231
Heavy Atom Count:20
Complexity:359

Purity/Quality:

99% ^*data from raw suppliers

4-NITROBENZO-2',3'-XYLIDIDE 95.00% ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC1=C(C(=CC=C1)NC(=O)C2=CC=C(C=C2)[N+](=O)[O-])C

Technology Process of N-(2,3-dimethylphenyl)-4-nitrobenzamide

There total 1 articles about N-(2,3-dimethylphenyl)-4-nitrobenzamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 122-04-3
4-nitro-benzoyl chloride

: 87-59-2
2,3-Dimethylaniline

: 35709-76-3
N-(2,3-dimethyl-phenyl)-4-nitro-benzamide

Guidance literature:: With 4-methyl-morpholine; In dichloromethane; at 0 - 20 ℃;
DOI:10.1016/S0968-0896(99)00165-0

Reference yield:

: 35709-76-3
N-(2,3-dimethyl-phenyl)-4-nitro-benzamide

: 29027-72-3
4-Aminobenzoesaeure-(2.3-dimethylanilid)

Guidance literature:: With tin(ll) chloride; In ethyl acetate; for 2h; Heating;
DOI:10.1016/S0968-0896(99)00165-0

Reference yield:

: 35709-76-3
N-(2,3-dimethyl-phenyl)-4-nitro-benzamide

: 3-[(3-tert-butyloxycarbonylaminopropionyl)amino]-N-(2,3-dimethylphenyl)-benzamide

Guidance literature:: Multi-step reaction with 2 steps

1.1: SnCl₂*H₂O / ethyl acetate / 2 h / Heating

2.1: isobutyl chloroformate; NMM / dimethylformamide / 0.08 h / -15 °C

2.2: dimethylformamide / -15 - 20 °C

With 4-methyl-morpholine; tin(ll) chloride; isobutyl chloroformate; In ethyl acetate; N,N-dimethyl-formamide; 1.1: Reduction / 2.1: Acylation / 2.2: Substitution;
DOI:10.1016/S0968-0896(99)00165-0