((C₆H₅)2PCH₂)3BC₆H₅^(1-)*(C₄H₉)4N⁽¹⁺⁾=[(C₄H₉)4N][((C₆H₅)2PCH₂)3BC₆H₅]

Base Information

Chemical Name:((C₆H₅)2PCH₂)3BC₆H₅^(1-)*(C₄H₉)4N⁽¹⁺⁾=[(C₄H₉)4N][((C₆H₅)2PCH₂)3BC₆H₅]
CAS No.:694484-07-6
Molecular Formula:C₁₆H₃₆N*C₄₅H₄₁BP₃
Molecular Weight:928.021
Hs Code.:

((C<sub>6</sub>H<sub>5</sub>)2PCH<sub>2</sub>)3BC<sub>6</sub>H<sub>5</sub><sup>(1-)</sup>*(C<sub>4</sub>H<sub>9</sub>)4N<sup>(1+)</sup>=[(C<sub>4</sub>H<sub>9</sub>)4N][((C<sub>6</sub>H<sub>5</sub>)2PCH<sub>2</sub>)3BC<sub>6</sub>H<sub>5</sub>]

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Chemical Property of ((C₆H₅)2PCH₂)3BC₆H₅^(1-)*(C₄H₉)4N⁽¹⁺⁾=[(C₄H₉)4N][((C₆H₅)2PCH₂)3BC₆H₅]

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Technology Process of ((C₆H₅)2PCH₂)3BC₆H₅^(1-)*(C₄H₉)4N⁽¹⁺⁾=[(C₄H₉)4N][((C₆H₅)2PCH₂)3BC₆H₅]

There total 1 articles about ((C₆H₅)2PCH₂)3BC₆H₅^(1-)*(C₄H₉)4N⁽¹⁺⁾=[(C₄H₉)4N][((C₆H₅)2PCH₂)3BC₆H₅] which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 67.3%

: 1643-19-2
tetrabutylammomium bromide

: 251460-45-4
Tris(diphenylphosphinomethyl)phenylborate

: 694484-07-6
((C₆H₅)2PCH₂)3BC₆H₅^(1-)*(C₄H₉)4N⁽¹⁺⁾=[(C₄H₉)4N][((C₆H₅)2PCH₂)3BC₆H₅]

Guidance literature:: With air; In methanol; water; Li-compd. was dissolved in MeOH in air, soln. was filtered via diatomaceous earth, Bu4NBr was added in H2O; solid was taken with addn. of Et2O, stirring (5 min), filtration, washing twice sequentially with H2O, Et2O, solid was dissolved iN MeCN, dried with Na2SO4 (stirring for 10 min with it), soln. was filtered, triturated with Et2O, elem. anal.;
DOI:10.1016/j.poly.2003.11.036

Reference yield: 90.3%

: (1,5-cyclooctadiene)dimethylplatinum(II)

: 694484-07-6
((C₆H₅)2PCH₂)3BC₆H₅^(1-)*(C₄H₉)4N⁽¹⁺⁾=[(C₄H₉)4N][((C₆H₅)2PCH₂)3BC₆H₅]

: 694484-12-3
[[κ(2)-PhB(CH2PPh2)3]PtMe2]Bu4N

Guidance literature:: In tetrahydrofuran; under N2, 1 equiv. of Pt-compd. in THF was added to THF soln. of B-compd., stirring for 4 h at room temp.; volatiles were removed, pptn. with pentane, solid was triturated with pentane, drying in vac., elem. anal.;
DOI:10.1016/j.poly.2003.11.036

Reference yield: 73.5%

: 694484-07-6
((C₆H₅)2PCH₂)3BC₆H₅^(1-)*(C₄H₉)4N⁽¹⁺⁾=[(C₄H₉)4N][((C₆H₅)2PCH₂)3BC₆H₅]

: 14364-93-3
trimethylplatinum(IV) iodide

: 694484-09-8
(κ(3)-(Ph2PCH2)3BPhPtMe3)

Guidance literature:: In tetrahydrofuran; byproducts: Bu4NI; under N2, Pt- and B-compds. were dissolved in THF, stirring for 2 h; soln. was concd., solid was pptd. upon standing, dried in vac., benzene was added, stirring for 10 min, soln. was filtered, volatiles were removed in vac., elem. anal.;
DOI:10.1016/j.poly.2003.11.036