Se-phenyl 3-((1,2-dimethyl-1,2,5,6-tetrahydro-3-pyridyl)methyl)-1H-2-indolecarboselenoate

Base Information

Chemical Name:Se-phenyl 3-((1,2-dimethyl-1,2,5,6-tetrahydro-3-pyridyl)methyl)-1H-2-indolecarboselenoate
CAS No.:878003-42-0
Molecular Formula:C₂₃H₂₄N₂OSe
Molecular Weight:423.416
Hs Code.:

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Se-phenyl 3-((1,2-dimethyl-1,2,5,6-tetrahydro-3-pyridyl)methyl)-1H-2-indolecarboselenoate

Chemical Property:

Purity/Quality:

Safty Information:

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MSDS Files:: SDS file from LookChem

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Technology Process of Se-phenyl 3-((1,2-dimethyl-1,2,5,6-tetrahydro-3-pyridyl)methyl)-1H-2-indolecarboselenoate

There total 1 articles about Se-phenyl 3-((1,2-dimethyl-1,2,5,6-tetrahydro-3-pyridyl)methyl)-1H-2-indolecarboselenoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 3-(1,2-dimethyl-1,2,5,6-tetrahydro-pyridin-3-ylmethyl)-1H-indole-2-carboxylic acid; compound with triethyl-amine

: 5707-04-0
Phenylselenyl chloride

: 878003-42-0
Se-phenyl 3-((1,2-dimethyl-1,2,5,6-tetrahydro-3-pyridyl)methyl)-1H-2-indolecarboselenoate

Guidance literature:: With tributylphosphine; In tetrahydrofuran; at 20 ℃;
DOI:10.1021/jo052428s

Reference yield: 75.0%

: 878003-42-0
Se-phenyl 3-((1,2-dimethyl-1,2,5,6-tetrahydro-3-pyridyl)methyl)-1H-2-indolecarboselenoate

: 878003-43-1
1,2-dimethyl-1,2,3,4,4a,6,11,11a-octahydro-pyrido[4,3-b]carbazol-5-one

Guidance literature:: With 2,2'-azobis(isobutyronitrile); tri-n-butyl-tin hydride; In benzene; for 3h; Heating;
DOI:10.1021/jo052428s

Reference yield:

: 878003-42-0
Se-phenyl 3-((1,2-dimethyl-1,2,5,6-tetrahydro-3-pyridyl)methyl)-1H-2-indolecarboselenoate

: 2744-45-8,11046-16-5
(+/-)-guatambuine

Guidance literature:: Multi-step reaction with 3 steps

1: 75 percent / n-Bu₃SnH; AIBN / benzene / 3 h / Heating

2: tetrahydrofuran; diethyl ether / 3 h / 20 °C

3: 32 mg / trifluoroacetic acid / Pd/C / 3 h / 20 °C

With 2,2'-azobis(isobutyronitrile); tri-n-butyl-tin hydride; trifluoroacetic acid; palladium on activated charcoal; In tetrahydrofuran; diethyl ether; benzene;
DOI:10.1021/jo052428s