[OsCl(η**(6)-p-cymene)(CH3NHNH2)(PPh(OEt)2](BPh4)

Base Information

Chemical Name:[OsCl(η**(6)-p-cymene)(CH3NHNH2)(PPh(OEt)2](BPh4)
CAS No.:1351192-36-3
Molecular Formula:C₂₁H₃₅ClN₂O₂OsP*C₂₄H₂₀B
Molecular Weight:923.382
Hs Code.:

Synonyms:

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Chemical Property of [OsCl(η**(6)-p-cymene)(CH3NHNH2)(PPh(OEt)2](BPh4)

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Technology Process of [OsCl(η**(6)-p-cymene)(CH3NHNH2)(PPh(OEt)2](BPh4)

There total 2 articles about [OsCl(η**(6)-p-cymene)(CH3NHNH2)(PPh(OEt)2](BPh4) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 1359766-94-1
[OsCl(η²-CH₂=CH₂)(η⁶-p-cymene){phenyldiethoxyphosphine}]BPh₄

: 60-34-4
methylhydrazine

: 1351192-36-3
[OsCl(η**(6)-p-cymene)(CH3NHNH2)(PPh(OEt)2](BPh4)

Guidance literature:: In dichloromethane; to soln. of Os complex added excess of CH3NHNH2; stirred at room temp. for 2 h; solvent removed under reduced pressure; oil treated with EtOH contg. excess NaBPh4; solid filtered, crystd. from CH2Cl2 and EtOH;
DOI:10.1016/j.jorganchem.2011.12.032

Reference yield: 71.0%

: 1219623-11-6
[OsCl₂(η⁶-p-cymene){PPh(OEt)₂}]

: 143-66-8
sodium tetraphenyl borate

: 60-34-4
methylhydrazine

: 1351192-36-3
[OsCl(η**(6)-p-cymene)(CH3NHNH2)(PPh(OEt)2](BPh4)

Guidance literature:: In ethanol; dichloromethane; N2 or Ar; EtOH/DCM (3/5, v/v) soln. of Ru compd. and NaBPh4 cooled to -196°C, ligand added (1:2:1.05 molar ratio), mixt. warmed to room temp., stirred for 5 h; evad. (vac.), triturated (EtOH), cooled to -25°C, septd., crystd.(EtOH), elem. anal.;
DOI:10.1016/j.jorganchem.2011.09.011

Reference yield: 63.0%

: 1174671-12-5
[RuCl2(η6-p-cymene)(P(OC2H5)2C6H5)]

: 1351192-36-3
[OsCl(η**(6)-p-cymene)(CH3NHNH2)(PPh(OEt)2](BPh4)

: 546-67-8
lead(IV) tetraacetate

: 1351192-46-5
[(η6-p-cymene)Os(P(OEt)2Ph)(N2Me)][BPh4]

Guidance literature:: In ethanol; dichloromethane; Ar or N2, DCM soln. of Ru compd. cooled to -30°C, Pb(OAc)4 added,warmed to 0°C, stirred for 5 min, evapd., triturated with EtOH s oln. of NaBPh4 (1:1.1.05:1 molar ratio), stirred at 0°C; septd., crystd. (DCM, EtOH), elem. anal.;
DOI:10.1016/j.jorganchem.2011.09.011