trichlorotris(tetrahydrofuran)molybdenum(III)

Base Information

Chemical Name:trichlorotris(tetrahydrofuran)molybdenum(III)
CAS No.:39210-30-5
Molecular Formula:C₁₂H₂₄Cl₃MoO₃
Molecular Weight:418.62
Hs Code.:

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of trichlorotris(tetrahydrofuran)molybdenum(III)

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Technology Process of trichlorotris(tetrahydrofuran)molybdenum(III)

There total 9 articles about trichlorotris(tetrahydrofuran)molybdenum(III) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

: 109-99-9,24979-97-3,77392-70-2
tetrahydrofuran

: 16998-75-7
tetrachlorobis(tetrahydrofurano)molybdenum(IV)

: 31355-55-2,39210-30-5
trichlorotris(tetrahydrofuran)molybdenum(III)

Guidance literature:: With tin; for 0.5h; Inert atmosphere;
DOI:10.15227/orgsyn.084.0163

Reference yield: 85.0%

: 10241-05-1
molybdenum(V) chloride

: 31355-55-2,39210-30-5
trichlorotris(tetrahydrofuran)molybdenum(III)

Guidance literature:: With tetrahydrofuran; In tetrahydrofuran; byproducts: H2, (C6H5)2SiHCl; dissolution of Ph2SiH2 in THF, slow addn. of MoCl5 with rapid stirring at room temp. (under dry N2, over ca. 20 min), gas evolution, further stirring for 4 h, forming a red-brown suspn.; filtn., washing twice with THF, elem. anal.;
DOI:10.1016/S0277-5387(00)80226-0

Reference yield: 82.0%

: 109-99-9,24979-97-3,77392-70-2
tetrahydrofuran

: 7440-31-5
tin

: 10241-05-1
molybdenum(V) chloride

: 31355-55-2,39210-30-5
trichlorotris(tetrahydrofuran)molybdenum(III)

Guidance literature:: In tetrahydrofuran; diethyl ether; under Ar; MoCl5 and Sn suspd. in Et2O, mixt. stirred for 30 min at room temp., liquid decanted off, THF added, mixt. stirred for 3 h at room temp.; excess Sn sepd. by transferring the gently stirred supernatant suspn. ina new flask, suspn. filtered, ppt. washed with Et2O, dried in vac.; ele m. anal.;
DOI:10.1002/1099-0682(200109)2001:10<2699::aid-ejic2699>3.0.co;2-s