Ru[((n)C₄H₉NH)2-glyoximato]2(dichloroglyoximato)(BC₆H₅)2

Base Information

Chemical Name:Ru[((n)C₄H₉NH)2-glyoximato]2(dichloroglyoximato)(BC₆H₅)2
CAS No.:439595-37-6
Molecular Formula:C₃₄H₅₀B₂Cl₂N₁₀O₆Ru
Molecular Weight:888.432
Hs Code.:

Ru[((n)C<sub>4</sub>H<sub>9</sub>NH)2-glyoximato]2(dichloroglyoximato)(BC<sub>6</sub>H<sub>5</sub>)2

Synonyms:

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Chemical Property of Ru[((n)C₄H₉NH)2-glyoximato]2(dichloroglyoximato)(BC₆H₅)2

Chemical Property:

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Technology Process of Ru[((n)C₄H₉NH)2-glyoximato]2(dichloroglyoximato)(BC₆H₅)2

There total 3 articles about Ru[((n)C₄H₉NH)2-glyoximato]2(dichloroglyoximato)(BC₆H₅)2 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 19.0%

: 439595-25-2
ruthenium(II)(dichloroglyoxime)3(BC₆H₅)2

: 109-73-9,85404-21-3
N-butylamine

: 439595-37-6
Ru[((n)C₄H₉NH)2-glyoximato]2(dichloroglyoximato)(BC₆H₅)2

Guidance literature:: In N,N-dimethyl-formamide; to a stirring soln./suspn. of Ru-contg. compd. in DMF was added dropwisea soln. of a 2-fold excess of n-butylamine in DMF for 2 h at -5° C; the mixt. was left overnight at room temp.; stirring at room temp. for 10 h; pptn. with a 2-fold vol. of H2O; solid was filtered, dried in vac., and dissolved in CHCl3; soln. was filtered through a Silasorb SPH-300 layer,dild. with hexane, and evapd. to dryness; the solid was washed with hex ane and dried in vac.; elem. anal.;
DOI:10.1039/b107172f

Reference yield:

: 3262-89-3
triphenylboroxine

: 439595-37-6
Ru[((n)C₄H₉NH)2-glyoximato]2(dichloroglyoximato)(BC₆H₅)2

Guidance literature:: Multi-step reaction with 2 steps

1: SbCl₃; Pb / chloroform; nitromethane

2: N,N-dimethyl-formamide

With SbCl₃; Pb; In nitromethane; chloroform; N,N-dimethyl-formamide;
DOI:10.1039/b107172f

Reference yield:

: 99177-32-9
i-C₄H₉OBClC₆H₅

: 439595-37-6
Ru[((n)C₄H₉NH)2-glyoximato]2(dichloroglyoximato)(BC₆H₅)2

Guidance literature:: Multi-step reaction with 2 steps

1: Pb / chloroform; nitromethane

2: N,N-dimethyl-formamide

With Pb; In nitromethane; chloroform; N,N-dimethyl-formamide;
DOI:10.1039/b107172f