C₂₃H₃₆O₃

Base Information

Chemical Name:C₂₃H₃₆O₃
CAS No.:1130279-41-2
Molecular Formula:C₂₃H₃₆O₃
Molecular Weight:360.537
Hs Code.:

C<sub>23</sub>H<sub>36</sub>O<sub>3</sub>

Synonyms:

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Chemical Property of C₂₃H₃₆O₃

Chemical Property:

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Technology Process of C₂₃H₃₆O₃

There total 18 articles about C₂₃H₃₆O₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

: 1130279-31-0
C₂₁H₃₂O₃

: 115-11-7,15220-85-6
isobutene

: 1130279-41-2
C₂₃H₃₆O₃

Guidance literature:: With tricyclohexylphosphine[1,3-bis(2,4,6-trimethylphenyl)-4,5-dihydroimidazol-2-ylidine][benzylidene]ruthenium(II) dichloride; In dichloromethane; at 50 ℃; for 72h; Sealed tube;

Reference yield:

: 1130279-45-6
C₁₆H₂₆O₄

: 1130279-41-2
C₂₃H₃₆O₃

Guidance literature:: Multi-step reaction with 14 steps

1.1: n-butyllithium / tetrahydrofuran / 0.17 h / -78 °C

1.2: -78 - 0 °C

2.1: manganese(IV) oxide / dichloromethane / 25 °C

3.1: triethylsilane; boron trifluoride diethyl etherate / dichloromethane / 2 h / -78 - -20 °C

4.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 1 h / 25 °C

5.1: pyridine; hydrogen / ethyl acetate / 3 h / 25 °C

6.1: hydrogenchloride; water / tetrahydrofuran / 3 h / 60 °C

7.1: sodium hydride / tetrahydrofuran / 1 h / Reflux

7.2: 4 h / 25 °C

8.1: sodium tetrahydroborate / ethanol / 0.5 h / 0 °C

8.2: 0.5 h / 0 - 25 °C

9.1: sodium tetrahydroborate / ethanol / 1 h / 0 °C

10.1: dmap; triethylamine / dichloromethane / 0.5 h / 0 - 25 °C

11.1: copper(I) iodide-lithium chloride / tetrahydrofuran; diethyl ether / 0.17 h / 25 °C

11.2: 0.5 h / 25 °C

12.1: Jones reagent / acetone / 0.5 h / 25 °C

13.1: potassium carbonate / N,N-dimethyl-formamide / 2 h / 25 °C

14.1: tricyclohexylphosphine[1,3-bis(2,4,6-trimethylphenyl)-4,5-dihydroimidazol-2-ylidine][benzylidene]ruthenium(II) dichloride / dichloromethane / 72 h / 50 °C

With pyridine; tricyclohexylphosphine[1,3-bis(2,4,6-trimethylphenyl)-4,5-dihydroimidazol-2-ylidine][benzylidene]ruthenium(II) dichloride; hydrogenchloride; triethylsilane; dmap; manganese(IV) oxide; sodium tetrahydroborate; Jones reagent; n-butyllithium; copper(I) iodide-lithium chloride; boron trifluoride diethyl etherate; tetrabutyl ammonium fluoride; water; hydrogen; sodium hydride; potassium carbonate; triethylamine; In tetrahydrofuran; diethyl ether; ethanol; dichloromethane; ethyl acetate; N,N-dimethyl-formamide; acetone;
DOI:10.1002/asia.201000147

Reference yield:

: 136598-01-1
(4aS,5S,6S,8aS)-(-)-2,4,4a,5,6,7,8,8a-Octahydro-6-hydroxy-5,8a-dimethyl-5-(prop-2-enyl)naphthalen-1(2H)-one 1-(Ethylene Acetal)

: 1130279-41-2
C₂₃H₃₆O₃

Guidance literature:: Multi-step reaction with 15 steps

1.1: ozone / ethyl acetate / 0.08 h / -78 °C

1.2: 6 h / 25 °C

2.1: n-butyllithium / tetrahydrofuran / 0.17 h / -78 °C

2.2: -78 - 0 °C

3.1: manganese(IV) oxide / dichloromethane / 25 °C

4.1: triethylsilane; boron trifluoride diethyl etherate / dichloromethane / 2 h / -78 - -20 °C

5.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 1 h / 25 °C

6.1: pyridine; hydrogen / ethyl acetate / 3 h / 25 °C

7.1: hydrogenchloride; water / tetrahydrofuran / 3 h / 60 °C

8.1: sodium hydride / tetrahydrofuran / 1 h / Reflux

8.2: 4 h / 25 °C

9.1: sodium tetrahydroborate / ethanol / 0.5 h / 0 °C

9.2: 0.5 h / 0 - 25 °C

10.1: sodium tetrahydroborate / ethanol / 1 h / 0 °C

11.1: dmap; triethylamine / dichloromethane / 0.5 h / 0 - 25 °C

12.1: copper(I) iodide-lithium chloride / tetrahydrofuran; diethyl ether / 0.17 h / 25 °C

12.2: 0.5 h / 25 °C

13.1: Jones reagent / acetone / 0.5 h / 25 °C

14.1: potassium carbonate / N,N-dimethyl-formamide / 2 h / 25 °C

15.1: tricyclohexylphosphine[1,3-bis(2,4,6-trimethylphenyl)-4,5-dihydroimidazol-2-ylidine][benzylidene]ruthenium(II) dichloride / dichloromethane / 72 h / 50 °C

With pyridine; tricyclohexylphosphine[1,3-bis(2,4,6-trimethylphenyl)-4,5-dihydroimidazol-2-ylidine][benzylidene]ruthenium(II) dichloride; hydrogenchloride; triethylsilane; dmap; manganese(IV) oxide; sodium tetrahydroborate; Jones reagent; n-butyllithium; copper(I) iodide-lithium chloride; boron trifluoride diethyl etherate; tetrabutyl ammonium fluoride; water; hydrogen; sodium hydride; potassium carbonate; ozone; triethylamine; In tetrahydrofuran; diethyl ether; ethanol; dichloromethane; ethyl acetate; N,N-dimethyl-formamide; acetone;
DOI:10.1002/asia.201000147