fac-[PtH(Ph₂PCH₂CH₂PPh₂)Me₃]

Base Information

Chemical Name:fac-[PtH(Ph₂PCH₂CH₂PPh₂)Me₃]
CAS No.:592472-31-6
Molecular Formula:C₂₉H₃₄P₂Pt
Molecular Weight:639.616
Hs Code.:

fac-[PtH(Ph<sub>2</sub>PCH<sub>2</sub>CH<sub>2</sub>PPh<sub>2</sub>)Me<sub>3</sub>]

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Chemical Property of fac-[PtH(Ph₂PCH₂CH₂PPh₂)Me₃]

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Technology Process of fac-[PtH(Ph₂PCH₂CH₂PPh₂)Me₃]

There total 1 articles about fac-[PtH(Ph₂PCH₂CH₂PPh₂)Me₃] which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 220197-83-1
fac-[bis(diphenylphosphino)ethane]PtMe₃(OAc)

: 25895-60-7
sodium cyanoborohydride

: 15630-18-9
cis-PtMe2(1,2-bis(diphenylphosphino)ethane)

: 592472-31-6
fac-[PtH(Ph₂PCH₂CH₂PPh₂)Me₃]

Guidance literature:: In tetrahydrofuran; under N2; NaCNBH3 added to soln. of fac-(Ph2PCH2CH2PPh2)PtMe3(OAc) in THF, stirred for 15 min; volatiles removed under vac., oily residue treated with Et2O, Et2O soln.evapd. under vac., residue rinsed with Et2O, soln. filtered, filtrate e vapd. under vac., recrystd. from Et2O/pentane;
DOI:10.1021/ja029140u

Reference yield:

: 592472-31-6
fac-[PtH(Ph₂PCH₂CH₂PPh₂)Me₃]

: 15630-18-9
cis-PtMe2(1,2-bis(diphenylphosphino)ethane)

Guidance literature:: In benzene-d6; byproducts: methane; thermolysis in soln. at 50°C; not isolated, detected by NMR spectroscopy; Kinetics;
DOI:10.1021/ja029140u