2-<2-phenyl>-1,3-bis(methylsulfonyloxy)propane

Base Information

Chemical Name:2-<2-phenyl>-1,3-bis(methylsulfonyloxy)propane
CAS No.:118481-27-9
Molecular Formula:C₁₃H₂₁NO₁₀S₄
Molecular Weight:479.574
Hs Code.:

2-<2-<bis(methylsulfonyl)amino>phenyl>-1,3-bis(methylsulfonyloxy)propane

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2-<2-phenyl>-1,3-bis(methylsulfonyloxy)propane

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Technology Process of 2-<2-phenyl>-1,3-bis(methylsulfonyloxy)propane

There total 1 articles about 2-<2-phenyl>-1,3-bis(methylsulfonyloxy)propane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 3.0%

: 124-63-0
methanesulfonyl chloride

: 54892-85-2
2-(2-aminophenyl)-1,3-propanediol

: 115875-74-6
1-methylsulfonyl-2-(methylsulfonyloxymethyl)indoline

: 118481-27-9
2-<2-phenyl>-1,3-bis(methylsulfonyloxy)propane

Guidance literature:: With triethylamine; In dichloromethane; for 3h; Ambient temperature;
DOI:10.1246/bcsj.61.310

Reference yield:

: 118481-27-9
2-<2-phenyl>-1,3-bis(methylsulfonyloxy)propane

: 118481-30-4
1-(methanesulfonyl)-1H-indole-3-carboxaldehyde

Guidance literature:: Multi-step reaction with 4 steps

1: 90 percent / ascorbic acid, anthracene / dimethylformamide / 2.4 h / Ambient temperature; cathodic electrolysis

2: 94 percent / 1,8-diazabicyclo<5.4.0>undec-7-ene / CH₂Cl₂ / 15 h / Heating

3: 85 percent / NaBr / acetonitrile; H₂O / 2.8 h / Ambient temperature; electrolysis

4: 80 percent / RuCl₂(PPh₃)3, O₂ / 1,2-dichloro-ethane / 4 h / 50 - 60 °C

With tris(triphenylphosphine)ruthenium(II) chloride; anthracene; oxygen; 1,8-diazabicyclo[5.4.0]undec-7-ene; sodium bromide; ascorbic acid; In dichloromethane; water; 1,2-dichloro-ethane; N,N-dimethyl-formamide; acetonitrile;
DOI:10.1246/bcsj.61.310