Butanoic acid, 3-oxo-, 1-phenylcyclohexyl ester

Base Information

• Chemical Name: Butanoic acid, 3-oxo-, 1-phenylcyclohexyl ester
• CAS No.: 139313-44-3
• Molecular Formula: C16H20O3
• Molecular Weight: 260.333
• Mol file: 139313-44-3.mol

Synonyms:

Chemical Property of Butanoic acid, 3-oxo-, 1-phenylcyclohexyl ester

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of Butanoic acid, 3-oxo-, 1-phenylcyclohexyl ester

There total 2 articles about Butanoic acid, 3-oxo-, 1-phenylcyclohexyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 61.0%

1-phenylcyclohexanol (1589-60-2) → 1-Phenylcyclohexene (771-98-2) + phenylcyclohexylacetate (26524-28-7) + 1'-phenylcyclohexyl 3-oxobutanoate (139313-44-3) + dimethylglyoxal (431-03-8)

Guidance literature:

With acetic anhydride; cobalt(II) chloride; In acetonitrile; at 80 ℃; for 10h;

DOI:10.1021/jo00033a020

Reference yield: 18.0%

1-phenylcyclohexanol (1589-60-2) + acetic anhydride (108-24-7) → 1-Phenylcyclohexene (771-98-2) + phenylcyclohexylacetate (26524-28-7) + 1'-phenylcyclohexyl 3-oxobutanoate (139313-44-3) + dimethylglyoxal (431-03-8)

Guidance literature:

With cobalt(II) chloride; In acetonitrile; at 80 ℃; for 10h;

DOI:10.1021/jo00033a020

upstream raw materials:

1-phenylcyclohexanol

acetic anhydride