C₂₈H₃₆O₉

Base Information

Chemical Name:C₂₈H₃₆O₉
CAS No.:1616470-02-0
Molecular Formula:C₂₈H₃₆O₉
Molecular Weight:516.588
Hs Code.:

C<sub>28</sub>H<sub>36</sub>O<sub>9</sub>

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₂₈H₃₆O₉

Chemical Property:

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Technology Process of C₂₈H₃₆O₉

There total 9 articles about C₂₈H₃₆O₉ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1616470-00-8
C₂₁H₃₂O₈

: 707-07-3
orthobenzoic acid trimethyl ester

: 1616470-02-0
C₂₈H₃₆O₉

: 1616470-04-2
(2R,3S)-1-ethoxy-3-hydroxy-4-((4R,5R)-5-(2-(4-methoxybenzyloxy)ethyl)-2,2-dimethyl-1,3-dioxolan-4-yl)-1-oxobutan-2-yl benzoate

Guidance literature:: With toluene-4-sulfonic acid; In dichloromethane; water; at 20 ℃; Overall yield = 88 %; Overall yield = 3.17 g; regioselective reaction;
DOI:10.1002/anie.201402440

Reference yield:

: 29311-53-3
(E)-3-hexene-1,6-dioic acid

: 1616470-02-0
C₂₈H₃₆O₉

Guidance literature:: Multi-step reaction with 8 steps

1.1: acetyl chloride / 0.08 h / -5 °C / Inert atmosphere

1.2: 100 °C / Inert atmosphere

2.1: AD-mix β; methanesulfonamide; sodium hydrogencarbonate / water; tert-butyl alcohol / 0 °C

3.1: toluene-4-sulfonic acid / 20 °C / Molecular sieve

4.1: lithium aluminium tetrahydride / tetrahydrofuran; diethyl ether / 0 - 30 °C

5.1: manganese(IV) oxide / 1,2-dichloro-ethane / 0.83 h / 62 °C

6.1: lanthanum(lll) triflate / toluene / 2 h / 20 °C

7.1: AD-mix β; methanesulfonamide / water; tert-butyl alcohol / 0 - 20 °C

8.1: toluene-4-sulfonic acid / water; dichloromethane / 20 °C

With manganese(IV) oxide; lithium aluminium tetrahydride; methanesulfonamide; AD-mix β; sodium hydrogencarbonate; toluene-4-sulfonic acid; acetyl chloride; lanthanum(lll) triflate; In tetrahydrofuran; diethyl ether; dichloromethane; water; 1,2-dichloro-ethane; toluene; tert-butyl alcohol; 2.1: |Sharpless Dihydroxylation / 5.1: |Wittig Olefination / 7.1: |Sharpless Dihydroxylation;
DOI:10.1002/anie.201402440

Reference yield:

: 273220-58-9
diisopropyl (3R,4R)-3,4-isopropylidenehexane-1,6-dioate

: 1616470-02-0
C₂₈H₃₆O₉

Guidance literature:: Multi-step reaction with 5 steps

1: lithium aluminium tetrahydride / tetrahydrofuran; diethyl ether / 0 - 30 °C

2: manganese(IV) oxide / 1,2-dichloro-ethane / 0.83 h / 62 °C

3: lanthanum(lll) triflate / toluene / 2 h / 20 °C

4: AD-mix β; methanesulfonamide / water; tert-butyl alcohol / 0 - 20 °C

5: toluene-4-sulfonic acid / water; dichloromethane / 20 °C

With manganese(IV) oxide; lithium aluminium tetrahydride; methanesulfonamide; AD-mix β; toluene-4-sulfonic acid; lanthanum(lll) triflate; In tetrahydrofuran; diethyl ether; dichloromethane; water; 1,2-dichloro-ethane; toluene; tert-butyl alcohol; 2: |Wittig Olefination / 4: |Sharpless Dihydroxylation;
DOI:10.1002/anie.201402440