2-allyl-N,N-dimethylbenzamide

Base Information

Chemical Name:2-allyl-N,N-dimethylbenzamide
CAS No.:117195-26-3
Molecular Formula:C₁₂H₁₅NO
Molecular Weight:189.257
Hs Code.:

Synonyms:

Suppliers and Price of 2-allyl-N,N-dimethylbenzamide

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

AK Scientific
2-Allyl-N,N-dimethylbenzamide
1g
$ 937.00

Total 2 raw suppliers

Chemical Property of 2-allyl-N,N-dimethylbenzamide

Chemical Property:

Purity/Quality:

97% ^*data from raw suppliers

2-Allyl-N,N-dimethylbenzamide ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of 2-allyl-N,N-dimethylbenzamide

There total 5 articles about 2-allyl-N,N-dimethylbenzamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 31.0%

: 107-18-6
allyl alcohol

: 611-74-5
N,N-dimethylbenzamide

: 117195-26-3
2-allyl-N,N-dimethylbenzamide

Guidance literature:: With carbonyl(pentamethylcyclopentadienyl)cobalt diiodide; silver(I) acetate; silver(I) triflimide; at 80 ℃; for 24h; Inert atmosphere; Glovebox;
DOI:10.1021/acs.orglett.6b00846

Reference yield:

: 35466-83-2
allyl methyl carbonate

: 611-74-5
N,N-dimethylbenzamide

: C₁₂H₁₅NO

: 117195-26-3
2-allyl-N,N-dimethylbenzamide

Guidance literature:: With silver hexafluoroantimonate; [ruthenium(II)(η⁶-1-methyl-4-isopropyl-benzene)(chloride)(μ-chloride)]₂; copper diacetate; In tetrahydrofuran; at 80 ℃; for 20h; Overall yield = 52 %; regioselective reaction; Sealed tube;
DOI:10.1039/c4cc03354j

Reference yield:

: 65-85-0,8013-63-6
benzoic acid

: C₁₂H₁₅NO

: 117195-26-3
2-allyl-N,N-dimethylbenzamide

Guidance literature:: Multi-step reaction with 3 steps

1: thionyl chloride / dichloromethane / 1 h / 0 - 20 °C

2: triethylamine / dichloromethane / 20 °C

3: [ruthenium(II)(η⁶-1-methyl-4-isopropyl-benzene)(chloride)(μ-chloride)]₂; silver hexafluoroantimonate; copper diacetate / tetrahydrofuran / 20 h / 80 °C / Sealed tube

With silver hexafluoroantimonate; thionyl chloride; [ruthenium(II)(η⁶-1-methyl-4-isopropyl-benzene)(chloride)(μ-chloride)]₂; copper diacetate; triethylamine; In tetrahydrofuran; dichloromethane;
DOI:10.1039/c4cc03354j