cis-thymidine 3',5'-cyclic phenyl phosphite

Base Information

Chemical Name:cis-thymidine 3',5'-cyclic phenyl phosphite
CAS No.:87970-10-3
Molecular Formula:C₁₆H₁₇N₂O₆P
Molecular Weight:364.295
Hs Code.:

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of cis-thymidine 3',5'-cyclic phenyl phosphite

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Technology Process of cis-thymidine 3',5'-cyclic phenyl phosphite

There total 3 articles about cis-thymidine 3',5'-cyclic phenyl phosphite which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 36.0%

: 40652-74-2,66512-18-3,66512-19-4
thymidine 3',5'-cyclic N,N-dimethylaminophosphoramidite

: 108-95-2,27073-41-2
phenol

: 87970-09-0,87970-10-3
cis-thymidine 3',5'-cyclic phenyl phosphite

Guidance literature:: With carbon dioxide; N,N-dimethylammonium chloride; In dichloromethane; for 2h;
DOI:10.1021/ja00247a036

Reference yield:

: 40652-74-2,66512-18-3,66512-19-4
thymidine 3',5'-cyclic N,N-dimethylaminophosphoramidite

: 108-95-2,27073-41-2
phenol

: 87970-10-3,87970-09-0
5-Methyl-1-((2R,4aR,6R,7aS)-2-phenoxy-tetrahydro-furo[3,2-d][1,3,2]dioxaphosphinin-6-yl)-1H-pyrimidine-2,4-dione

: 87970-09-0,87970-10-3
cis-thymidine 3',5'-cyclic phenyl phosphite

Guidance literature:: With pyridine hydrochloride; In dichloromethane; at -10 ℃; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
DOI:10.1021/ja00364a052

Reference yield:

: 40652-74-2,66512-18-3,66512-19-4
thymidine 3',5'-cyclic N,N-dimethylaminophosphoramidite

: 108-95-2,27073-41-2
phenol

: 87970-10-3,87970-09-0
5-Methyl-1-((2R,4aR,6R,7aS)-2-phenoxy-tetrahydro-furo[3,2-d][1,3,2]dioxaphosphinin-6-yl)-1H-pyrimidine-2,4-dione

: 87970-09-0,87970-10-3
cis-thymidine 3',5'-cyclic phenyl phosphite

Guidance literature:: With pyridine hydrochloride; In dichloromethane; at -10 ℃; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
DOI:10.1021/ja00364a052