((C₆H₅)3P)2N⁽¹⁺⁾*S₃N₃O₂^(1-)=(((C₆H₅)3P)2N)S₃N₃O₂

Base Information

• Chemical Name: ((C₆H₅)3P)2N⁽¹⁺⁾*S₃N₃O₂^(1-)=(((C₆H₅)3P)2N)S₃N₃O₂
• CAS No.: 86176-90-1
• Molecular Formula: C₃₆H₃₀NP₂*N₃O₂S₃
• Molecular Weight: 708.805

Synonyms:

Chemical Property of ((C₆H₅)3P)2N⁽¹⁺⁾*S₃N₃O₂^(1-)=(((C₆H₅)3P)2N)S₃N₃O₂

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Technology Process of ((C₆H₅)3P)2N⁽¹⁺⁾*S₃N₃O₂^(1-)=(((C₆H₅)3P)2N)S₃N₃O₂

There total 3 articles about ((C₆H₅)3P)2N⁽¹⁺⁾*S₃N₃O₂^(1-)=(((C₆H₅)3P)2N)S₃N₃O₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 79.0%

S4N4O2 + bis(triphenylphosphorylidene)ammonium azide (38011-36-8) → ((C6H5)3P)2N(1+)*S3N3O2(1-)=(((C6H5)3P)2N)S3N3O2 (86176-90-1)

Guidance literature:

In acetonitrile; byproducts: N2, S8; (((C6H5)3P)2N)N3 added to S4N4O2 slurry under N2, stirred and heated toreflux for 3 h; cooled to -20°C for 2 h, crystals extd. (Et2O), recrystd. (hot MeCN); elem. anal.;

Reference yield: 60.0%

C36H30NP2(1+)*N5O2S4(1-) → ((C6H5)3P)2N(1+)*S3N3O2(1-)=(((C6H5)3P)2N)S3N3O2 (86176-90-1)

Guidance literature:

In acetonitrile; Product distribution; Heating;

DOI:10.1039/c39870000110

Reference yield:

bis(triphenylphosphine)iminium trisulfur trinitride → ((C6H5)3P)2N(1+)*S4N5O(1-)=(((C6H5)3P)2N)S4N5O (86163-11-3) + bis(triphenylphosphine)iminium tetrasulfur pentanitride (72884-88-9) + ((C6H5)3P)2N(1+)*S3N3O2(1-)=(((C6H5)3P)2N)S3N3O2 (86176-90-1)

Guidance literature:

With O₂; In acetonitrile; (((C6H5)3P)2N)S3N3 slurry allowed to react with atm. O2 by slow diffusion for 24 h; concd., cooled to -20°C overnight, filtered, concd. (vac.), cooled to -20°C for 24 h;

upstream raw materials:

bis(triphenylphosphorylidene)ammonium azide

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