3-methyl-4-bromo benzophenone

Base Information

Chemical Name:3-methyl-4-bromo benzophenone
CAS No.:85588-37-0
Molecular Formula:C₁₄H₁₁BrO
Molecular Weight:275.145
Hs Code.:

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 3-methyl-4-bromo benzophenone

Chemical Property:

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Technology Process of 3-methyl-4-bromo benzophenone

There total 5 articles about 3-methyl-4-bromo benzophenone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 77.4%

: 21900-25-4
4-bromo-3-methylbenzoyl chloride

: 71-43-2,26181-88-4,54682-86-9,13967-78-7,174973-66-1
benzene

: 85588-37-0
3-methyl-4-bromo benzophenone

Guidance literature:: With aluminium trichloride; for 3h; Heating;

Reference yield:

: 98-88-4
benzoyl chloride

: 202865-85-8
1-bromo-4-iodo-2-methylbenzene

: 85588-37-0
3-methyl-4-bromo benzophenone

Guidance literature:: 1-bromo-4-iodo-2-methylbenzene; With isopropylmagnesium chloride; In tetrahydrofuran; at -78 ℃; for 3h; Inert atmosphere;

With copper (I) cyanide di(lithium chloride)complex; In tetrahydrofuran; at -78 ℃; Inert atmosphere;

benzoyl chloride; In tetrahydrofuran; at -78 - 20 ℃; Inert atmosphere;
DOI:10.1039/c3cc49313j

Reference yield:

: 13194-68-8
4-iodo-2-methylaniline

: 85588-37-0
3-methyl-4-bromo benzophenone

Guidance literature:: Multi-step reaction with 2 steps

1.1: copper(ll) bromide; n-Butyl nitrite / acetonitrile / 65 °C

2.1: isopropylmagnesium chloride / tetrahydrofuran / 3 h / -78 °C / Inert atmosphere

2.2: -78 °C / Inert atmosphere

2.3: -78 - 20 °C / Inert atmosphere

With n-Butyl nitrite; isopropylmagnesium chloride; copper(ll) bromide; In tetrahydrofuran; acetonitrile;
DOI:10.1039/c3cc49313j