2-dimethylsila 1,3-diphenyl 1,3-diphospholane

Base Information

Chemical Name:2-dimethylsila 1,3-diphenyl 1,3-diphospholane
CAS No.:53088-58-7
Molecular Formula:C₁₆H₂₀P₂Si
Molecular Weight:302.368
Hs Code.:

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Chemical Property of 2-dimethylsila 1,3-diphenyl 1,3-diphospholane

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Technology Process of 2-dimethylsila 1,3-diphenyl 1,3-diphospholane

There total 1 articles about 2-dimethylsila 1,3-diphenyl 1,3-diphospholane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 53088-58-7,57733-92-3,57733-98-9
2-dimethylsila 1,3-diphenyl 1,3-diphospholane

Guidance literature:: PhHP(CH2)2PHPh, Na, Me2SiCl2;
DOI:10.1002/zaac.19744060209

Reference yield: 64.0%

: (x)C₄H₈O₂*(x)Cl₂Ge

: 53088-58-7,57733-92-3,57733-98-9
2-dimethylsila 1,3-diphenyl 1,3-diphospholane

: 63746-62-3,63746-64-5,81744-44-7
germylene 2-germanium(II) 1,3-diphenyl 1,3-diphospholane

Guidance literature:: In tetrahydrofuran; benzene; byproducts: (CH3)2SiCl2; under Ar, soln. of phosholane in benzene reacted with soln. of Ge-compd. in THF, 24 h; solvents, (CH3)2Cl2 and dioxane removed, dissolved in toluene, filtered;