Ethyl-o-nitro-benzolsulfinat

Base Information

Chemical Name:Ethyl-o-nitro-benzolsulfinat
CAS No.:49558-57-8
Molecular Formula:C₈H₉NO₄S
Molecular Weight:215.23
Hs Code.:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Ethyl-o-nitro-benzolsulfinat

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Technology Process of Ethyl-o-nitro-benzolsulfinat

There total 4 articles about Ethyl-o-nitro-benzolsulfinat which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 27489-28-7
methyl 2-(2-nitrophenylsulfonyl)acetate

: 49558-57-8
Ethyl-o-nitro-benzolsulfinat

Guidance literature:: Multi-step reaction with 2 steps

1: N₂H₄*H₂O / methanol / -10 °C

2: (i) aq. HCl, AcOH, NaNO₂, (ii) /BRN= 1718733/

With hydrazine hydrate; In methanol;
DOI:10.1021/jo00917a031

Reference yield:

: 58534-21-7
2-Nitro-benzenesulfinic acid 1-phenyl-meth-(Z)-ylideneamide

: 49558-57-8
Ethyl-o-nitro-benzolsulfinat

Guidance literature:: Multi-step reaction with 2 steps

1: Si₂Me₆ / Heating

2: H₂O

With 1,1,1,2,2,2-hexamethyldisilane; water;
DOI:10.1021/jo00867a039