7-chloro-N-(1-(7-chloro-6-fluorobenzo[d]thiazol-2-yl)-5-(4-(dimethylamino)phenyl)-4,5-dihydro-1H-pyrazol-3-yl)-6-fluoro-5-nitrobenzo[d]thiazol-2-amine

Base Information

Chemical Name:7-chloro-N-(1-(7-chloro-6-fluorobenzo[d]thiazol-2-yl)-5-(4-(dimethylamino)phenyl)-4,5-dihydro-1H-pyrazol-3-yl)-6-fluoro-5-nitrobenzo[d]thiazol-2-amine
CAS No.:1367374-89-7
Molecular Formula:C₂₅H₁₇Cl₂F₂N₇O₂S₂
Molecular Weight:620.49
Hs Code.:

7-chloro-N-(1-(7-chloro-6-fluorobenzo[d]thiazol-2-yl)-5-(4-(dimethylamino)phenyl)-4,5-dihydro-1H-pyrazol-3-yl)-6-fluoro-5-nitrobenzo[d]thiazol-2-amine

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Chemical Property of 7-chloro-N-(1-(7-chloro-6-fluorobenzo[d]thiazol-2-yl)-5-(4-(dimethylamino)phenyl)-4,5-dihydro-1H-pyrazol-3-yl)-6-fluoro-5-nitrobenzo[d]thiazol-2-amine

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Technology Process of 7-chloro-N-(1-(7-chloro-6-fluorobenzo[d]thiazol-2-yl)-5-(4-(dimethylamino)phenyl)-4,5-dihydro-1H-pyrazol-3-yl)-6-fluoro-5-nitrobenzo[d]thiazol-2-amine

There total 5 articles about 7-chloro-N-(1-(7-chloro-6-fluorobenzo[d]thiazol-2-yl)-5-(4-(dimethylamino)phenyl)-4,5-dihydro-1H-pyrazol-3-yl)-6-fluoro-5-nitrobenzo[d]thiazol-2-amine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 77.0%

: 218155-19-2
7-chloro-6-fluoro-2-hydrazinylbenzo[d]thiazole

: 1367374-77-3
N-(7-chloro-6-fluoro-5-nitrobenzo[d]thiazol-2-yl)-3-(4-(dimethylamino)phenyl)acrylamide

: 1367374-89-7
7-chloro-N-(1-(7-chloro-6-fluorobenzo[d]thiazol-2-yl)-5-(4-(dimethylamino)phenyl)-4,5-dihydro-1H-pyrazol-3-yl)-6-fluoro-5-nitrobenzo[d]thiazol-2-amine

Guidance literature:: With acetic acid; In ethanol; for 8h; Reflux;
DOI:10.1002/ardp.201100072

Reference yield:

: 367-21-5
3-chloro-4-fluorophenylamine

: 1367374-89-7
7-chloro-N-(1-(7-chloro-6-fluorobenzo[d]thiazol-2-yl)-5-(4-(dimethylamino)phenyl)-4,5-dihydro-1H-pyrazol-3-yl)-6-fluoro-5-nitrobenzo[d]thiazol-2-amine

Guidance literature:: Multi-step reaction with 3 steps

1: bromine; acetic acid / 14 h / 5 - 20 °C

2: hydrogenchloride; hydrazine hydrate / water; ethylene glycol / 2 h / 5 - 10 °C / Reflux

3: acetic acid / ethanol / 8 h / Reflux

With hydrogenchloride; bromine; hydrazine hydrate; acetic acid; In ethanol; water; ethylene glycol;
DOI:10.1002/ardp.201100072

Reference yield:

: 101337-93-3
2-amino-6-fluoro-7-chloro-1,3-benzothiazole

: 1367374-89-7
7-chloro-N-(1-(7-chloro-6-fluorobenzo[d]thiazol-2-yl)-5-(4-(dimethylamino)phenyl)-4,5-dihydro-1H-pyrazol-3-yl)-6-fluoro-5-nitrobenzo[d]thiazol-2-amine

Guidance literature:: Multi-step reaction with 2 steps

1: hydrogenchloride; hydrazine hydrate / water; ethylene glycol / 2 h / 5 - 10 °C / Reflux

2: acetic acid / ethanol / 8 h / Reflux

With hydrogenchloride; hydrazine hydrate; acetic acid; In ethanol; water; ethylene glycol;
DOI:10.1002/ardp.201100072