N-n-butylbenzophenoneimine(pentacarbonyl)tungsten

Base Information

• Chemical Name: N-n-butylbenzophenoneimine(pentacarbonyl)tungsten
• CAS No.: 99536-48-8
• Molecular Formula: C₂₂H₁₉NO₅W
• Molecular Weight: 561.247
• Mol file: 99536-48-8.mol

Synonyms:

Chemical Property of N-n-butylbenzophenoneimine(pentacarbonyl)tungsten

Chemical Property:

Purity/Quality:

Safty Information:

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MSDS Files:

Useful:

Technology Process of N-n-butylbenzophenoneimine(pentacarbonyl)tungsten

There total 1 articles about N-n-butylbenzophenoneimine(pentacarbonyl)tungsten which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 41.0%

pentacarbonyl(diphenylcarben)wolfram + t-butyl azide (13686-33-4) → N-n-butylbenzophenoneimine(pentacarbonyl)tungsten (99536-48-8)

Guidance literature:

In dichloromethane; byproducts: N2; N-BuN3 was added dropwise to a CH2Cl2 soln. of W-complex at room temp. under N2, mixt. was stirred for 5 min; chromd. over Kieselgel with pentane at -20°C, eluate evapd. under high vac., residue recrystd. from pentane; elem. anal.;

DOI:10.1016/0022-328X(85)88006-2

upstream raw materials:

t-butyl azide