N-(t-butoxycarbonyl)-O-benzyl-L-serine N-hydroxy-5-norbornene-2,3-dicarboximide ester

Base Information

Chemical Name:N-(t-butoxycarbonyl)-O-benzyl-L-serine N-hydroxy-5-norbornene-2,3-dicarboximide ester
CAS No.:76398-77-1
Molecular Formula:C₂₄H₂₈N₂O₇
Molecular Weight:456.496
Hs Code.:

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N-(t-butoxycarbonyl)-O-benzyl-L-serine N-hydroxy-5-norbornene-2,3-dicarboximide ester

Chemical Property:

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Technology Process of N-(t-butoxycarbonyl)-O-benzyl-L-serine N-hydroxy-5-norbornene-2,3-dicarboximide ester

There total 1 articles about N-(t-butoxycarbonyl)-O-benzyl-L-serine N-hydroxy-5-norbornene-2,3-dicarboximide ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 21715-90-2
N-hydroxy-5-norbornene-2,3-dicarboximide

: 23680-31-1
BOC-O-benzyl-L-serine

: 76398-77-1
N-(t-butoxycarbonyl)-O-benzyl-L-serine N-hydroxy-5-norbornene-2,3-dicarboximide ester

Guidance literature:: With dicyclohexyl-carbodiimide; In N,N-dimethyl-formamide; acetonitrile; 1.) 0 deg C, 1 h, 2.) RT, 4 h;
DOI:10.1246/bcsj.53.2570

Reference yield:

: 76398-77-1
N-(t-butoxycarbonyl)-O-benzyl-L-serine N-hydroxy-5-norbornene-2,3-dicarboximide ester

: 71921-84-1
O-benzyl-L-seryl-D-isoglutamine benzyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: acetonitrile / 15 h / Ambient temperature

2: CF₃COOH / 0.33 h / Ambient temperature

With trifluoroacetic acid; In acetonitrile;
DOI:10.1246/bcsj.53.2570

Reference yield:

: 76398-77-1
N-(t-butoxycarbonyl)-O-benzyl-L-serine N-hydroxy-5-norbornene-2,3-dicarboximide ester

: 76379-13-0
(R)-4-((S)-3-Benzyloxy-2-{(R)-2-[(4aR,6S,7R,8R,8aS)-6-benzyloxy-7-(2-benzyloxy-acetylamino)-2-phenyl-hexahydro-pyrano[3,2-d][1,3]dioxin-8-yloxy]-propionylamino}-propionylamino)-4-carbamoyl-butyric acid benzyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: acetonitrile / 15 h / Ambient temperature

2: CF₃COOH / 0.33 h / Ambient temperature

3: acetonitrile / 15 h / Ambient temperature

With trifluoroacetic acid; In acetonitrile;
DOI:10.1246/bcsj.53.2570