(1S,4S,6S)-6-(1-Benzenesulfonyl-1H-indol-2-yl)-2-aza-bicyclo[2.2.2]oct-7-ene-2,6-dicarboxylic acid 6-methyl ester 2-(2,2,2-trichloro-ethyl) ester

Base Information

Chemical Name:(1S,4S,6S)-6-(1-Benzenesulfonyl-1H-indol-2-yl)-2-aza-bicyclo[2.2.2]oct-7-ene-2,6-dicarboxylic acid 6-methyl ester 2-(2,2,2-trichloro-ethyl) ester
CAS No.:79328-90-8
Molecular Formula:C₂₆H₂₃Cl₃N₂O₆S
Molecular Weight:597.903
Hs Code.:

(1S,4S,6S)-6-(1-Benzenesulfonyl-1H-indol-2-yl)-2-aza-bicyclo[2.2.2]oct-7-ene-2,6-dicarboxylic acid 6-methyl ester 2-(2,2,2-trichloro-ethyl) ester

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (1S,4S,6S)-6-(1-Benzenesulfonyl-1H-indol-2-yl)-2-aza-bicyclo[2.2.2]oct-7-ene-2,6-dicarboxylic acid 6-methyl ester 2-(2,2,2-trichloro-ethyl) ester

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Technology Process of (1S,4S,6S)-6-(1-Benzenesulfonyl-1H-indol-2-yl)-2-aza-bicyclo[2.2.2]oct-7-ene-2,6-dicarboxylic acid 6-methyl ester 2-(2,2,2-trichloro-ethyl) ester

There total 1 articles about (1S,4S,6S)-6-(1-Benzenesulfonyl-1H-indol-2-yl)-2-aza-bicyclo[2.2.2]oct-7-ene-2,6-dicarboxylic acid 6-methyl ester 2-(2,2,2-trichloro-ethyl) ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 13.0%

: 66531-21-3
1-<(2,2,2-trichloroethoxy)carbonyl>-1,2-dihydropyridine

: 74185-41-4
methyl α-methylene-1-(phenylsulfonyl)-1H-indole-2-acetate

: 79328-90-8
(1S,4S,6S)-6-(1-Benzenesulfonyl-1H-indol-2-yl)-2-aza-bicyclo[2.2.2]oct-7-ene-2,6-dicarboxylic acid 6-methyl ester 2-(2,2,2-trichloro-ethyl) ester

Guidance literature:: at 100 ℃; for 48h;
DOI:10.1021/jo00337a003

Reference yield:

: 79-22-1
methyl chloroformate

: 79328-90-8
(1S,4S,6S)-6-(1-Benzenesulfonyl-1H-indol-2-yl)-2-aza-bicyclo[2.2.2]oct-7-ene-2,6-dicarboxylic acid 6-methyl ester 2-(2,2,2-trichloro-ethyl) ester

: 74195-04-3
(1S,4S,6S)-6-(1-Benzenesulfonyl-1H-indol-2-yl)-2-aza-bicyclo[2.2.2]oct-7-ene-2,6-dicarboxylic acid dimethyl ester

Guidance literature:: With acetic acid; triethylamine; zinc; Yield given. Multistep reaction; 1) 0 deg C, 2) ether, 15 min;
DOI:10.1021/jo00337a003