(3aR,4S,6S,7S,7aS)-6-((3aR,4S,6R,7S,7aR)-6-Benzyloxy-2,2,4-trimethyl-tetrahydro-[1,3]dioxolo[4,5-c]pyran-7-yloxy)-2,2,4-trimethyl-tetrahydro-[1,3]dioxolo[4,5-c]pyran-7-ylamine

Base Information

Chemical Name:(3aR,4S,6S,7S,7aS)-6-((3aR,4S,6R,7S,7aR)-6-Benzyloxy-2,2,4-trimethyl-tetrahydro-[1,3]dioxolo[4,5-c]pyran-7-yloxy)-2,2,4-trimethyl-tetrahydro-[1,3]dioxolo[4,5-c]pyran-7-ylamine
CAS No.:1053248-04-6
Molecular Formula:C₂₅H₃₇NO₈
Molecular Weight:479.571
Hs Code.:

(3aR,4S,6S,7S,7aS)-6-((3aR,4S,6R,7S,7aR)-6-Benzyloxy-2,2,4-trimethyl-tetrahydro-[1,3]dioxolo[4,5-c]pyran-7-yloxy)-2,2,4-trimethyl-tetrahydro-[1,3]dioxolo[4,5-c]pyran-7-ylamine

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Suppliers and Price of (3aR,4S,6S,7S,7aS)-6-((3aR,4S,6R,7S,7aR)-6-Benzyloxy-2,2,4-trimethyl-tetrahydro-[1,3]dioxolo[4,5-c]pyran-7-yloxy)-2,2,4-trimethyl-tetrahydro-[1,3]dioxolo[4,5-c]pyran-7-ylamine

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Chemical Property of (3aR,4S,6S,7S,7aS)-6-((3aR,4S,6R,7S,7aR)-6-Benzyloxy-2,2,4-trimethyl-tetrahydro-[1,3]dioxolo[4,5-c]pyran-7-yloxy)-2,2,4-trimethyl-tetrahydro-[1,3]dioxolo[4,5-c]pyran-7-ylamine

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Technology Process of (3aR,4S,6S,7S,7aS)-6-((3aR,4S,6R,7S,7aR)-6-Benzyloxy-2,2,4-trimethyl-tetrahydro-[1,3]dioxolo[4,5-c]pyran-7-yloxy)-2,2,4-trimethyl-tetrahydro-[1,3]dioxolo[4,5-c]pyran-7-ylamine

There total 5 articles about (3aR,4S,6S,7S,7aS)-6-((3aR,4S,6R,7S,7aR)-6-Benzyloxy-2,2,4-trimethyl-tetrahydro-[1,3]dioxolo[4,5-c]pyran-7-yloxy)-2,2,4-trimethyl-tetrahydro-[1,3]dioxolo[4,5-c]pyran-7-ylamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 208467-66-7
benzyl 2-azido-2-deoxy-3,4-O-isopropylidene-α-L-fucopyranosyl-(1-2)-3,4-O-isopropylidene-α-L-fucopyranoside

: 1053248-04-6
(3aR,4S,6S,7S,7aS)-6-((3aR,4S,6R,7S,7aR)-6-Benzyloxy-2,2,4-trimethyl-tetrahydro-[1,3]dioxolo[4,5-c]pyran-7-yloxy)-2,2,4-trimethyl-tetrahydro-[1,3]dioxolo[4,5-c]pyran-7-ylamine

Guidance literature:: With lithium aluminium tetrahydride; In tetrahydrofuran; at 20 ℃; for 1h;

Reference yield:

: 71731-75-4
benzyl 3,4-O-isopropylidene-α-L-fucopyranoside

: 1053248-04-6
(3aR,4S,6S,7S,7aS)-6-((3aR,4S,6R,7S,7aR)-6-Benzyloxy-2,2,4-trimethyl-tetrahydro-[1,3]dioxolo[4,5-c]pyran-7-yloxy)-2,2,4-trimethyl-tetrahydro-[1,3]dioxolo[4,5-c]pyran-7-ylamine

Guidance literature:: Multi-step reaction with 4 steps

1: 73 percent / TMSOTf, mol sieves 4A / CH₂Cl₂ / 1 h

2: NaOMe, MeOH

3: H⁽¹⁺⁾ / CH₂Cl₂ / 2 h

4: LiAlH₄ / tetrahydrofuran / 1 h / 20 °C

With methanol; lithium aluminium tetrahydride; trimethylsilyl trifluoromethanesulfonate; 4 A molecular sieve; sodium methylate; hydrogen cation; In tetrahydrofuran; dichloromethane;

Reference yield:

: (2S,3S,4S,5S,6S)-5-Azido-6-((3aR,4S,6R,7S,7aR)-6-benzyloxy-2,2,4-trimethyl-tetrahydro-[1,3]dioxolo[4,5-c]pyran-7-yloxy)-2-methyl-tetrahydro-pyran-3,4-diol

: 1053248-04-6
(3aR,4S,6S,7S,7aS)-6-((3aR,4S,6R,7S,7aR)-6-Benzyloxy-2,2,4-trimethyl-tetrahydro-[1,3]dioxolo[4,5-c]pyran-7-yloxy)-2,2,4-trimethyl-tetrahydro-[1,3]dioxolo[4,5-c]pyran-7-ylamine

Guidance literature:: Multi-step reaction with 2 steps

1: H⁽¹⁺⁾ / CH₂Cl₂ / 2 h

2: LiAlH₄ / tetrahydrofuran / 1 h / 20 °C

With lithium aluminium tetrahydride; hydrogen cation; In tetrahydrofuran; dichloromethane;