N⁴-<2-Acetamido-4-O-(2-acetamido-3,4,6-tri-O-acetyl-2-desoxy-β-D-glucopyranosyl)-3,6-di-O-acetyl-2-desoxy-β-D-glucopyranosyl>-L-asparaginyl-L-phenylalanyl-L-treonin-allylester-trifluoracetat

Base Information

• Chemical Name: N⁴-<2-Acetamido-4-O-(2-acetamido-3,4,6-tri-O-acetyl-2-desoxy-β-D-glucopyranosyl)-3,6-di-O-acetyl-2-desoxy-β-D-glucopyranosyl>-L-asparaginyl-L-phenylalanyl-L-treonin-allylester-trifluoracetat
• CAS No.: 117143-01-8
• Molecular Formula: C₂HF₃O₂*C₄₆H₆₄N₆O₂₁
• Molecular Weight: 1151.07

Synonyms:

Chemical Property of N⁴-<2-Acetamido-4-O-(2-acetamido-3,4,6-tri-O-acetyl-2-desoxy-β-D-glucopyranosyl)-3,6-di-O-acetyl-2-desoxy-β-D-glucopyranosyl>-L-asparaginyl-L-phenylalanyl-L-treonin-allylester-trifluoracetat

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of N⁴-<2-Acetamido-4-O-(2-acetamido-3,4,6-tri-O-acetyl-2-desoxy-β-D-glucopyranosyl)-3,6-di-O-acetyl-2-desoxy-β-D-glucopyranosyl>-L-asparaginyl-L-phenylalanyl-L-treonin-allylester-trifluoracetat

There total 9 articles about N⁴-<2-Acetamido-4-O-(2-acetamido-3,4,6-tri-O-acetyl-2-desoxy-β-D-glucopyranosyl)-3,6-di-O-acetyl-2-desoxy-β-D-glucopyranosyl>-L-asparaginyl-L-phenylalanyl-L-treonin-allylester-trifluoracetat which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

2-acetamido-4-O-(2-acetamido-3,4,6-tri-O-acetyl-2-deoxy-β-D-glucopyranosyl)-3,6-di-O-acetyl-2-deoxy-α-D-glucopyranosyl chloride (7531-49-9) → N4-<2-Acetamido-4-O-(2-acetamido-3,4,6-tri-O-acetyl-2-desoxy-β-D-glucopyranosyl)-3,6-di-O-acetyl-2-desoxy-β-D-glucopyranosyl>-L-asparaginyl-L-phenylalanyl-L-treonin-allylester-trifluoracetat (117143-01-8)

Guidance literature:

Multi-step reaction with 6 steps

1: 75 percent / sodium azide, tricaprylmethylammonium chloride / H₂O; CHCl₃ / Ambient temperature

2: 60 percent / H₂ / PtO₂

3: 91 percent / EEDQ / CH₂Cl₂ / 72 h / Ambient temperature

4: 95 percent / morpholine / (Ph₃P)4Pd⁽⁰⁾ / tetrahydrofuran; dimethylsulfoxide / 4 h / Ambient temperature

5: 81 percent / triethylamine, EEDQ / dimethylformamide / 72 h / Ambient temperature

6: 9.1 mg / 1 h / Ambient temperature

With morpholine; sodium azide; hydrogen; Aliquat 336; N-ethoxycarbonyl-2-ethoxy-1,2-dihydroquinoline; triethylamine; platinum(IV) oxide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In tetrahydrofuran; dichloromethane; chloroform; water; dimethyl sulfoxide; N,N-dimethyl-formamide;

Reference yield:

2-acetamido-4-O-(2-acetamido-3,4,6-tri-O-acetyl-2-deoxy-β-D-glucopyranosyl)-3,6-di-O-acetyl-2-deoxy-β-D-glucopyranosylamine (29673-51-6) → N4-<2-Acetamido-4-O-(2-acetamido-3,4,6-tri-O-acetyl-2-desoxy-β-D-glucopyranosyl)-3,6-di-O-acetyl-2-desoxy-β-D-glucopyranosyl>-L-asparaginyl-L-phenylalanyl-L-treonin-allylester-trifluoracetat (117143-01-8)

Guidance literature:

Multi-step reaction with 4 steps

1: 91 percent / EEDQ / CH₂Cl₂ / 72 h / Ambient temperature

2: 95 percent / morpholine / (Ph₃P)4Pd⁽⁰⁾ / tetrahydrofuran; dimethylsulfoxide / 4 h / Ambient temperature

3: 81 percent / triethylamine, EEDQ / dimethylformamide / 72 h / Ambient temperature

4: 9.1 mg / 1 h / Ambient temperature

With morpholine; N-ethoxycarbonyl-2-ethoxy-1,2-dihydroquinoline; triethylamine; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In tetrahydrofuran; dichloromethane; dimethyl sulfoxide; N,N-dimethyl-formamide;

Reference yield:

2-acetamido-2-deoxy-3,4,6-tri-O-acetyl-β-D-glucopyranosyl-(1-4)-2-acetamido-2-deoxy-3,6-di-O-acetyl-β-D-glucopyranosyl azide (29625-70-5) → N4-<2-Acetamido-4-O-(2-acetamido-3,4,6-tri-O-acetyl-2-desoxy-β-D-glucopyranosyl)-3,6-di-O-acetyl-2-desoxy-β-D-glucopyranosyl>-L-asparaginyl-L-phenylalanyl-L-treonin-allylester-trifluoracetat (117143-01-8)

Guidance literature:

Multi-step reaction with 5 steps

1: 60 percent / H₂ / PtO₂

2: 91 percent / EEDQ / CH₂Cl₂ / 72 h / Ambient temperature

3: 95 percent / morpholine / (Ph₃P)4Pd⁽⁰⁾ / tetrahydrofuran; dimethylsulfoxide / 4 h / Ambient temperature

4: 81 percent / triethylamine, EEDQ / dimethylformamide / 72 h / Ambient temperature

5: 9.1 mg / 1 h / Ambient temperature

With morpholine; hydrogen; N-ethoxycarbonyl-2-ethoxy-1,2-dihydroquinoline; triethylamine; platinum(IV) oxide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In tetrahydrofuran; dichloromethane; dimethyl sulfoxide; N,N-dimethyl-formamide;

upstream raw materials:

2-acetamido-4-O-(2-acetamido-3,4,6-tri-O-acetyl-2-deoxy-β-D-glucopyranosyl)-3,6-di-O-acetyl-2-deoxy-α-D-glucopyranosyl chloride

N-tert-butoxycarbonyl-L-phenylalanine

2-acetamido-4-O-(2-acetamido-3,4,6-tri-O-acetyl-2-deoxy-β-D-glucopyranosyl)-3,6-di-O-acetyl-2-deoxy-β-D-glucopyranosylamine

2-acetamido-2-deoxy-3,4,6-tri-O-acetyl-β-D-glucopyranosyl-(1-4)-2-acetamido-2-deoxy-3,6-di-O-acetyl-β-D-glucopyranosyl azide

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