3-O-[(2'',3''-di-O-benzyl-4'',6''-O-benzylidene-β-D-galactopyranosyl)-(1->6)-(2',3',4'-tri-O-benzyl-β-D-galactopyranosyl)]-1,2-di-O-(4-methoxybenzyl)-sn-glycerol

Base Information

Chemical Name:3-O-[(2'',3''-di-O-benzyl-4'',6''-O-benzylidene-β-D-galactopyranosyl)-(1->6)-(2',3',4'-tri-O-benzyl-β-D-galactopyranosyl)]-1,2-di-O-(4-methoxybenzyl)-sn-glycerol
CAS No.:1114560-42-7
Molecular Formula:C₇₃H₇₈O₁₅
Molecular Weight:1195.41
Hs Code.:

3-O-[(2'',3''-di-O-benzyl-4'',6''-O-benzylidene-β-D-galactopyranosyl)-(1->6)-(2',3',4'-tri-O-benzyl-β-D-galactopyranosyl)]-1,2-di-O-(4-methoxybenzyl)-sn-glycerol

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Chemical Property of 3-O-[(2'',3''-di-O-benzyl-4'',6''-O-benzylidene-β-D-galactopyranosyl)-(1->6)-(2',3',4'-tri-O-benzyl-β-D-galactopyranosyl)]-1,2-di-O-(4-methoxybenzyl)-sn-glycerol

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Technology Process of 3-O-[(2'',3''-di-O-benzyl-4'',6''-O-benzylidene-β-D-galactopyranosyl)-(1->6)-(2',3',4'-tri-O-benzyl-β-D-galactopyranosyl)]-1,2-di-O-(4-methoxybenzyl)-sn-glycerol

There total 1 articles about 3-O-[(2'',3''-di-O-benzyl-4'',6''-O-benzylidene-β-D-galactopyranosyl)-(1->6)-(2',3',4'-tri-O-benzyl-β-D-galactopyranosyl)]-1,2-di-O-(4-methoxybenzyl)-sn-glycerol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1101186-12-2
o-methoxycarbonylphenyl 2,3-di-O-benzyl-4,6-O-benzylidene-1-thio-β-D-galactopyranoside

: 1114560-40-5
3-O-(2',3',4'-tri-O-benzyl-β-D-galactopyranosyl)-1,2-di-O-(4-methoxybenzyl)-sn-glycerol

: 1114560-42-7
3-O-[(2'',3''-di-O-benzyl-4'',6''-O-benzylidene-β-D-galactopyranosyl)-(1->6)-(2',3',4'-tri-O-benzyl-β-D-galactopyranosyl)]-1,2-di-O-(4-methoxybenzyl)-sn-glycerol

Guidance literature:: o-methoxycarbonylphenyl 2,3-di-O-benzyl-4,6-O-benzylidene-1-thio-β-D-galactopyranoside; 3-O-(2',3',4'-tri-O-benzyl-β-D-galactopyranosyl)-1,2-di-O-(4-methoxybenzyl)-sn-glycerol; In dichloromethane; acetonitrile; at 20 ℃; for 3h; Molecular sieve; Inert atmosphere;

With N-iodo-succinimide; In dichloromethane; acetonitrile; at -40 - 20 ℃; Inert atmosphere;

With trifluorormethanesulfonic acid; In dichloromethane; acetonitrile; at -40 ℃; for 0.5h; Inert atmosphere;
DOI:10.1016/j.carres.2008.09.028

Reference yield:

: 1114560-42-7
3-O-[(2'',3''-di-O-benzyl-4'',6''-O-benzylidene-β-D-galactopyranosyl)-(1->6)-(2',3',4'-tri-O-benzyl-β-D-galactopyranosyl)]-1,2-di-O-(4-methoxybenzyl)-sn-glycerol

: 1101186-21-3
C₅₇H₆₂O₁₃

Guidance literature:: With 2,3-dicyano-5,6-dichloro-p-benzoquinone; In dichloromethane; water; isopropyl alcohol; at 0 - 20 ℃; for 5h; Inert atmosphere;
DOI:10.1016/j.carres.2008.09.028