hexahydridotris(tricyclohexylphosphine)molybdenum(VI)

Base Information

Chemical Name:hexahydridotris(tricyclohexylphosphine)molybdenum(VI)
CAS No.:84430-71-7
Molecular Formula:C₅₄H₁₀₅MoP₃
Molecular Weight:943.289
Hs Code.:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of hexahydridotris(tricyclohexylphosphine)molybdenum(VI)

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Technology Process of hexahydridotris(tricyclohexylphosphine)molybdenum(VI)

There total 1 articles about hexahydridotris(tricyclohexylphosphine)molybdenum(VI) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 5.0%

: 16998-75-7
tetrachlorobis(tetrahydrofurano)molybdenum(IV)

: 22722-98-1
sodium bis(2-methoxyethoxy)aluminium dihydride

: 2622-14-2
tricyclohexylphosphine

: 84430-71-7
hexahydridotris(tricyclohexylphosphine)molybdenum(VI)

Guidance literature:: In tetrahydrofuran; Complex and phosphine were reflixed in THF for 15 min, cooled to-80°C, NaH2Al(OCH2CH2OCH3)2 soln. was added slowly, the mixt. was allowed to warm to room temp. and stirred overnight (Ar atm.);; evapd., Et2O was added, aq. NaOH was added, ether layer was dried with MgSO4, filtered, evapd. in vac.; ppt. was extd. with hexane, evapd.;;