Boc-PheΨGly-ACHPA-Leu-NHCH2-m-Ph-CH2NH2

Base Information

Chemical Name:Boc-PheΨGly-ACHPA-Leu-NHCH2-m-Ph-CH2NH2
CAS No.:118405-04-2
Molecular Formula:C₄₂H₆₅N₅O₇
Molecular Weight:752.007
Hs Code.:

Boc-PheΨ<CHOHCH2>Gly-ACHPA-Leu-NHCH2-m-Ph-CH2NH2

Synonyms:

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Chemical Property of Boc-PheΨGly-ACHPA-Leu-NHCH2-m-Ph-CH2NH2

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Technology Process of Boc-PheΨGly-ACHPA-Leu-NHCH2-m-Ph-CH2NH2

There total 6 articles about Boc-PheΨGly-ACHPA-Leu-NHCH2-m-Ph-CH2NH2 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 118405-01-9,124338-98-3,124339-26-0
Boc-PheΨACHPA-Leu-NHCH2-m-Ph-CH2NHZ

: 118405-04-2,124339-02-2,124339-32-8,151282-85-8
Boc-PheΨGly-ACHPA-Leu-NHCH2-m-Ph-CH2NH2

Guidance literature:: With hydrogen; nickel; In methanol; at 24 ℃; under 2585.7 Torr;
DOI:10.1021/jm00164a058

Reference yield:

: 99113-32-3,99113-34-5,118386-98-4
(2E,4R,S,5S)-5-<<(1,1-dimethylethoxy)carbonyl>amino>-4-hydroxy-6-phenyl-2-hexenoic acid

: 118405-04-2,124339-02-2,124339-32-8,151282-85-8
Boc-PheΨGly-ACHPA-Leu-NHCH2-m-Ph-CH2NH2

Guidance literature:: Multi-step reaction with 2 steps

1: HOBT/DCC, Et₃N / dimethylformamide / 1.) 0 deg C, 0.5 h, 2.) room temp.

2: H₂ / Raney Ni / methanol / 24 °C / 2585.7 Torr

With hydrogen; benzotriazol-1-ol; triethylamine; dicyclohexyl-carbodiimide; nickel; In methanol; N,N-dimethyl-formamide;
DOI:10.1021/jm00164a058

Reference yield:

: 118457-05-9
Methyl (S)-5-<(tert-butoxycarbonyl)amino>-6-phenyl-(E)-3-hexenoate

: 118405-04-2,124339-02-2,124339-32-8,151282-85-8
Boc-PheΨGly-ACHPA-Leu-NHCH2-m-Ph-CH2NH2

Guidance literature:: Multi-step reaction with 4 steps

1: 100 percent / m-chloroperbenzoic acid / CH₂Cl₂ / 72 h / Ambient temperature

2: 1.1 g / 1 N NaOH / methanol / 2 h / Ambient temperature

3: HOBT/DCC, Et₃N / dimethylformamide / 1.) 0 deg C, 0.5 h, 2.) room temp.

4: H₂ / Raney Ni / methanol / 24 °C / 2585.7 Torr

With sodium hydroxide; hydrogen; benzotriazol-1-ol; triethylamine; 3-chloro-benzenecarboperoxoic acid; dicyclohexyl-carbodiimide; nickel; In methanol; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1021/jm00164a058