(1S,3R,4S,5R,6R,7R)-1-((4S,5R)-4-Acetoxy-5-methyl-3-methylene-6-phenyl-hexyl)-6-((E)-(4S,6S)-4,6-dimethyl-oct-2-enoyloxy)-4-hydroxy-3-hydroxymethyl-7-(1-methoxy-1-methyl-ethoxy)-2,8-dioxa-bicyclo[3.2.1]octane-4,5-dicarboxylic acid di-tert-butyl ester

Base Information

Chemical Name:(1S,3R,4S,5R,6R,7R)-1-((4S,5R)-4-Acetoxy-5-methyl-3-methylene-6-phenyl-hexyl)-6-((E)-(4S,6S)-4,6-dimethyl-oct-2-enoyloxy)-4-hydroxy-3-hydroxymethyl-7-(1-methoxy-1-methyl-ethoxy)-2,8-dioxa-bicyclo[3.2.1]octane-4,5-dicarboxylic acid di-tert-butyl ester
CAS No.:154110-06-2
Molecular Formula:C₄₇H₇₂O₁₄
Molecular Weight:861.08
Hs Code.:

(1S,3R,4S,5R,6R,7R)-1-((4S,5R)-4-Acetoxy-5-methyl-3-methylene-6-phenyl-hexyl)-6-((E)-(4S,6S)-4,6-dimethyl-oct-2-enoyloxy)-4-hydroxy-3-hydroxymethyl-7-(1-methoxy-1-methyl-ethoxy)-2,8-dioxa-bicyclo[3.2.1]octane-4,5-dicarboxylic acid di-tert-butyl ester

Synonyms:

Suppliers and Price of (1S,3R,4S,5R,6R,7R)-1-((4S,5R)-4-Acetoxy-5-methyl-3-methylene-6-phenyl-hexyl)-6-((E)-(4S,6S)-4,6-dimethyl-oct-2-enoyloxy)-4-hydroxy-3-hydroxymethyl-7-(1-methoxy-1-methyl-ethoxy)-2,8-dioxa-bicyclo[3.2.1]octane-4,5-dicarboxylic acid di-tert-butyl ester

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of (1S,3R,4S,5R,6R,7R)-1-((4S,5R)-4-Acetoxy-5-methyl-3-methylene-6-phenyl-hexyl)-6-((E)-(4S,6S)-4,6-dimethyl-oct-2-enoyloxy)-4-hydroxy-3-hydroxymethyl-7-(1-methoxy-1-methyl-ethoxy)-2,8-dioxa-bicyclo[3.2.1]octane-4,5-dicarboxylic acid di-tert-butyl ester

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of (1S,3R,4S,5R,6R,7R)-1-((4S,5R)-4-Acetoxy-5-methyl-3-methylene-6-phenyl-hexyl)-6-((E)-(4S,6S)-4,6-dimethyl-oct-2-enoyloxy)-4-hydroxy-3-hydroxymethyl-7-(1-methoxy-1-methyl-ethoxy)-2,8-dioxa-bicyclo[3.2.1]octane-4,5-dicarboxylic acid di-tert-butyl ester

There total 5 articles about (1S,3R,4S,5R,6R,7R)-1-((4S,5R)-4-Acetoxy-5-methyl-3-methylene-6-phenyl-hexyl)-6-((E)-(4S,6S)-4,6-dimethyl-oct-2-enoyloxy)-4-hydroxy-3-hydroxymethyl-7-(1-methoxy-1-methyl-ethoxy)-2,8-dioxa-bicyclo[3.2.1]octane-4,5-dicarboxylic acid di-tert-butyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 71432-55-8
2-tert-butyl-1,3-diisopropylisourea

: 154110-06-2
(1S,3R,4S,5R,6R,7R)-1-((4S,5R)-4-Acetoxy-5-methyl-3-methylene-6-phenyl-hexyl)-6-((E)-(4S,6S)-4,6-dimethyl-oct-2-enoyloxy)-4-hydroxy-3-hydroxymethyl-7-(1-methoxy-1-methyl-ethoxy)-2,8-dioxa-bicyclo[3.2.1]octane-4,5-dicarboxylic acid di-tert-butyl ester

Guidance literature:: Multi-step reaction with 4 steps

1: 90 percent / CH₂Cl₂ / 3 h / 40 °C

2: 95 percent / PPTS / CH₂Cl₂ / 2 h / 0 °C

3: 98 percent / 2,5-dihydrotoluene / 10percent Pd/C / CH₂Cl₂ / 3 h / 40 °C

4: 1.) N-methylmorpholine, Cl-CO₂-iBu; 2.) NaBH₄ / 1.) CH₂Cl₂; 2.) MeOH

With 4-methyl-morpholine; sodium tetrahydroborate; 2,5-dihydrotoluene; isobutyl chloroformate; palladium on activated charcoal; pyridinium p-toluenesulfonate; In dichloromethane;
DOI:10.1016/S0040-4039(00)91815-X

Reference yield:

: 146006-63-5
(1S,3S,4S,5R,6R,7R)-1-((4S,5R)-4-Acetoxy-5-methyl-3-methylene-6-phenyl-hexyl)-6-((E)-(4S,6S)-4,6-dimethyl-oct-2-enoyloxy)-4,7-dihydroxy-2,8-dioxa-bicyclo[3.2.1]octane-3,4,5-tricarboxylic acid 3-benzyl ester 4,5-di-tert-butyl ester

: 154110-06-2
(1S,3R,4S,5R,6R,7R)-1-((4S,5R)-4-Acetoxy-5-methyl-3-methylene-6-phenyl-hexyl)-6-((E)-(4S,6S)-4,6-dimethyl-oct-2-enoyloxy)-4-hydroxy-3-hydroxymethyl-7-(1-methoxy-1-methyl-ethoxy)-2,8-dioxa-bicyclo[3.2.1]octane-4,5-dicarboxylic acid di-tert-butyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: 95 percent / PPTS / CH₂Cl₂ / 2 h / 0 °C

2: 98 percent / 2,5-dihydrotoluene / 10percent Pd/C / CH₂Cl₂ / 3 h / 40 °C

3: 1.) N-methylmorpholine, Cl-CO₂-iBu; 2.) NaBH₄ / 1.) CH₂Cl₂; 2.) MeOH

With 4-methyl-morpholine; sodium tetrahydroborate; 2,5-dihydrotoluene; isobutyl chloroformate; palladium on activated charcoal; pyridinium p-toluenesulfonate; In dichloromethane;
DOI:10.1016/S0040-4039(00)91815-X

Reference yield:

: 146006-47-5
(1S,3S,4S,5R,6R,7R)-1-((4S,5R)-4-Acetoxy-5-methyl-3-methylene-6-phenyl-hexyl)-6-((E)-(4S,6S)-4,6-dimethyl-oct-2-enoyloxy)-4,7-dihydroxy-2,8-dioxa-bicyclo[3.2.1]octane-3,4,5-tricarboxylic acid 3-benzyl ester

: 154110-06-2
(1S,3R,4S,5R,6R,7R)-1-((4S,5R)-4-Acetoxy-5-methyl-3-methylene-6-phenyl-hexyl)-6-((E)-(4S,6S)-4,6-dimethyl-oct-2-enoyloxy)-4-hydroxy-3-hydroxymethyl-7-(1-methoxy-1-methyl-ethoxy)-2,8-dioxa-bicyclo[3.2.1]octane-4,5-dicarboxylic acid di-tert-butyl ester

Guidance literature:: Multi-step reaction with 4 steps

1: 90 percent / CH₂Cl₂ / 3 h / 40 °C

2: 95 percent / PPTS / CH₂Cl₂ / 2 h / 0 °C

3: 98 percent / 2,5-dihydrotoluene / 10percent Pd/C / CH₂Cl₂ / 3 h / 40 °C

4: 1.) N-methylmorpholine, Cl-CO₂-iBu; 2.) NaBH₄ / 1.) CH₂Cl₂; 2.) MeOH

With 4-methyl-morpholine; sodium tetrahydroborate; 2,5-dihydrotoluene; isobutyl chloroformate; palladium on activated charcoal; pyridinium p-toluenesulfonate; In dichloromethane;
DOI:10.1016/S0040-4039(00)91815-X