(η2-bis(diphenylphosphino)methylamine)tricarbonylruthenium

Base Information

Chemical Name:(η2-bis(diphenylphosphino)methylamine)tricarbonylruthenium
CAS No.:297180-63-3
Molecular Formula:C₂₈H₂₃NO₃P₂Ru
Molecular Weight:584.513
Hs Code.:

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Chemical Property of (η2-bis(diphenylphosphino)methylamine)tricarbonylruthenium

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Technology Process of (η2-bis(diphenylphosphino)methylamine)tricarbonylruthenium

There total 2 articles about (η2-bis(diphenylphosphino)methylamine)tricarbonylruthenium which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 15243-33-1
dodecacarbonyl-triangulo-triruthenium

: 2960-43-2
bis(diphenylphosphino)methylamine

: 297180-63-3
(η2-bis(diphenylphosphino)methylamine)tricarbonylruthenium

Guidance literature:: With ethylene; In n-heptane; Irradiation (UV/VIS); under N2; the Ru compd. was dissolved in n-heptane, the soln. was bubbled with CH2CH2 for 30 min followed by irradiation for 15 min, the ligandwas added, the ethylene gas was removed under vac., the soln. was stirred overnight at 50°C; the soln. was concd., the product was pptd. with pentane and washed three times;
DOI:10.1021/om000289t

Reference yield:

: 297180-59-7
(η1-bis(diphenylphosphino)methylamine)tetracarbonylruthenium

: 297180-63-3
(η2-bis(diphenylphosphino)methylamine)tricarbonylruthenium

Guidance literature:: In n-heptane; under N2; in temp. controlled infrared cell; rate constants were determined by monitoring IR absorbances at temp. from 284.09 K to 313.48 K; not isolated, detected by NMR; Kinetics;
DOI:10.1021/om000289t

Reference yield:

: 297180-63-3
(η2-bis(diphenylphosphino)methylamine)tricarbonylruthenium

: Ru2(CO)4(μ2-P(C6H5)2)(μ-(C6H5)2PN(CH3)P(C6H5)2)(C(O)NCH3P(C6H5)2)

Guidance literature:: In dichloromethane; pentane; byproducts: CO; under N2; slow diffusion of pentane into a CH2Cl2 soln. of complex overa period of 1 m;
DOI:10.1021/om000289t