(+/-)-methyl dihydroepijasmonate

Base Information

Chemical Name:(+/-)-methyl dihydroepijasmonate
CAS No.:133163-97-0
Molecular Formula:C₁₃H₂₂O₃
Molecular Weight:226.316
Hs Code.:

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (+/-)-methyl dihydroepijasmonate

Chemical Property:

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Technology Process of (+/-)-methyl dihydroepijasmonate

There total 44 articles about (+/-)-methyl dihydroepijasmonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 24863-70-5
(3-oxo-2-pentyl-cyclopent-1-enyl)-acetic acid methyl ester

: 2570-03-8,2630-39-9,24851-98-7,39647-11-5,93452-03-0,133163-97-0,133163-98-1,128087-96-7
(+/-)-methyl dihydroepijasmonate

Guidance literature:: With hydrogen; palladium on activated charcoal; In methanol; for 24h; under 760 Torr; Ambient temperature;
DOI:10.1016/S0040-4039(00)88791-2

Reference yield: 93.0%

: 54562-27-5,84893-69-6,108102-95-0,109008-64-2,109361-58-2,109361-60-6,119009-18-6,119009-19-7,136845-16-4,143292-36-8,146143-16-0
((1R,2S,3R)-3-Hydroxy-2-pentyl-cyclopentyl)-acetic acid methyl ester

: 2570-03-8,2630-39-9,24851-98-7,39647-11-5,93452-03-0,133163-97-0,133163-98-1,128087-96-7
(+/-)-methyl dihydroepijasmonate

Guidance literature:: With dipyridinium dichromate; In dichloromethane; for 44h;

Reference yield:

: 25564-22-1
2-pentyl-2-cyclopenten-1-one

: 2570-03-8,2630-39-9,24851-98-7,39647-11-5,93452-03-0,133163-97-0,133163-98-1,128087-96-7
(+/-)-methyl dihydroepijasmonate

Guidance literature:: Multi-step reaction with 4 steps

1.1: LiCl; CuI / diethyl ether; tetrahydrofuran / 0.08 h / -80 °C

1.2: diethyl ether; tetrahydrofuran / 1 h / -80 - -30 °C

1.3: 70 percent / 2-(methyliminomethyl)phenol / diethyl ether; tetrahydrofuran / -80 - 20 °C

2.1: O₃ / CH₂Cl₂ / 0.25 h / -80 °C

2.2: 70 percent / Me₂S / CH₂Cl₂ / -80 - 20 °C

3.1: NaH₂PO₄*H₂O; 30percent H₂O₂; NaClO₂ / H₂O; acetonitrile / 24 h / 20 °C

4.1: diethyl ether; methanol / 0.5 h / 20 °C

With sodium chlorite; sodium dihydrogenphosphate; copper(l) iodide; ozone; lithium chloride; In tetrahydrofuran; methanol; diethyl ether; dichloromethane; water; acetonitrile;
DOI:10.1002/1099-0690(200110)2001:20<3837::AID-EJOC3837>3.0.CO;2-3