[Me2Al(μ-2,4,6-trimethylbenzoate)]2

Base Information

Chemical Name:[Me2Al(μ-2,4,6-trimethylbenzoate)]2
CAS No.:884337-83-1
Molecular Formula:C₂₄H₃₄Al₂O₄
Molecular Weight:440.495
Hs Code.:

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Chemical Property of [Me2Al(μ-2,4,6-trimethylbenzoate)]2

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Technology Process of [Me2Al(μ-2,4,6-trimethylbenzoate)]2

There total 1 articles about [Me2Al(μ-2,4,6-trimethylbenzoate)]2 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

: 480-63-7
mesitylenecarboxylic acid

: 75-24-1
trimethylaluminum

: 884337-83-1
[Me2Al(μ-2,4,6-trimethylbenzoate)]2

Guidance literature:: In hexane; byproducts: CH4; in a glovebox, Al-contg. compd. (2.00 mmol) was slowly added to a cooledhexane suspn. (-35.degree C) of carboxylic acid (2.00 mmol); stirring a t ambient temp. for 3 h; the solvent was removed in vac.; elem. anal.;
DOI:10.1021/om060052i

Reference yield: 80.0%

: tris(η2-tetramethylaluminato)yttrium(III)

: 884337-83-1
[Me2Al(μ-2,4,6-trimethylbenzoate)]2

: Y[(2,4,6-trimethylbenzoate)2(μ-AlMe2)]3

Guidance literature:: In hexane; toluene; in a glovebox, to a soln. of Y-contg. compd. (1.00 mmol) in hexane was slowly added a toluene soln. of (Me2Al(μ-O2CAr(Me))2 compd. (1.50 mmol); stirring overnight (18 h) at ambient temp.; the solvent was removed in vac.; extn. in toluene; the compd. was washedseveral times with hexane, dried until const. wt. under reduced pressur e; other compds. were also obtained;
DOI:10.1021/om060052i

Reference yield: 70.0%

: lanthanum tetramethylaluminate

: 884337-83-1
[Me2Al(μ-2,4,6-trimethylbenzoate)]2

: La(2,4,6-trimethylbenzoate)2(μ-AlMe2)]3

Guidance literature:: In hexane; toluene; in a glovebox, to a soln. of La-contg. compd. (1.00 mmol) in hexane was slowly added a toluene soln. of (Me2Al(μ-O2CAr(Me))2 compd. (1.50 mmol); stirring overnight (18 h) at ambient temp.; the solvent was removed in vac.; extn. in toluene; the compd. was washedseveral times with hexane, dried until const. wt. under reduced pressur e; other compds. were also obtained;
DOI:10.1021/om060052i