(cyclo-octa-1,5-diene)tris(hydrazine)hydridoruthenium tetraphenylborate

Base Information

Chemical Name:(cyclo-octa-1,5-diene)tris(hydrazine)hydridoruthenium tetraphenylborate
CAS No.:37726-72-0
Molecular Formula:C₈H₂₅N₆Ru*C₂₄H₂₀B
Molecular Weight:625.63
Hs Code.:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (cyclo-octa-1,5-diene)tris(hydrazine)hydridoruthenium tetraphenylborate

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Technology Process of (cyclo-octa-1,5-diene)tris(hydrazine)hydridoruthenium tetraphenylborate

There total 2 articles about (cyclo-octa-1,5-diene)tris(hydrazine)hydridoruthenium tetraphenylborate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 65390-74-1
(cyclo-octa-1,5-diene)tris(N',N'-dimethylhydrazine)hydridorutheniumtetraphenylborate

: 37726-72-0
(cyclo-octa-1,5-diene)tris(hydrazine)hydridoruthenium tetraphenylborate

Guidance literature:: With hydrazine; In methanol; excess hydrazine, refluxing for 15 min; slow addn. of water to hot soln., pptn. on cooling to room temp.; can berecrystallized (aq. MeOH contg. N2H4);
DOI:10.1039/DT9770001809

Reference yield: 50.0%

: dichloro(1,5-cyclooctadiene)ruthenium(II)

: 143-66-8
sodium tetraphenyl borate

: 37726-72-0
(cyclo-octa-1,5-diene)tris(hydrazine)hydridoruthenium tetraphenylborate

Guidance literature:: With methanol; water; hydrazine; In methanol; water; stirring Ru-complex with excess 97% N2H4 in MeOH to dissoln., water addn., refluxing for 2.5 h, addn. of excess aq. NaBPh4; crystn. (-5°C, several h); elem. anal.;
DOI:10.1039/DT9770001809