N,N,N-dipropylbenzylamine borane

Base Information

Chemical Name:N,N,N-dipropylbenzylamine borane
CAS No.:854204-51-6
Molecular Formula:C₁₃H₂₄BN
Molecular Weight:205.151
Hs Code.:

Synonyms:

Suppliers and Price of N,N,N-dipropylbenzylamine borane

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of N,N,N-dipropylbenzylamine borane

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of N,N,N-dipropylbenzylamine borane

There total 1 articles about N,N,N-dipropylbenzylamine borane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 25.0%

: 4856-92-2
benzylamine BH₃ adduct

: 107-08-4
1-iodo-propane

: 854204-41-4
N,N-propylbenzylamine borane

: 854204-51-6
N,N,N-dipropylbenzylamine borane

Guidance literature:: With s-butyllithium; In tetrahydrofuran; cyclohexane; (N2); dropwise addn. of a soln. of lithium compd. in cyclohexane to a soln. of boron compd. in THF at -78°C, stirring for 30 min, warmingto room temp. for 30 min, cooling to -78°C, addn. of alkyl iodid e, stirring for 1 h at room temp.; addn. of satd. NaHCO3, extn. aq. layer with ether, drying (Na2SO4), evapn., flash chromy. (silica gel, 10% ethyl acetate in petroleum ether); elem. anal.;
DOI:10.1016/j.jorganchem.2005.01.059