[1,2,4]Triazol-1-yl-phosphonic acid 2-chloro-phenyl ester (2R,3S,5R)-2-[(4-methoxy-phenyl)-diphenyl-methoxymethyl]-5-(5-methyl-2,4-dioxo-3,4-dihydro-2H-pyrimidin-1-yl)-tetrahydro-furan-3-yl ester

Base Information

Chemical Name:[1,2,4]Triazol-1-yl-phosphonic acid 2-chloro-phenyl ester (2R,3S,5R)-2-[(4-methoxy-phenyl)-diphenyl-methoxymethyl]-5-(5-methyl-2,4-dioxo-3,4-dihydro-2H-pyrimidin-1-yl)-tetrahydro-furan-3-yl ester
CAS No.:82892-62-4
Molecular Formula:C₃₈H₃₅ClN₅O₈P
Molecular Weight:756.151
Hs Code.:

[1,2,4]Triazol-1-yl-phosphonic acid 2-chloro-phenyl ester (2R,3S,5R)-2-[(4-methoxy-phenyl)-diphenyl-methoxymethyl]-5-(5-methyl-2,4-dioxo-3,4-dihydro-2H-pyrimidin-1-yl)-tetrahydro-furan-3-yl ester

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Chemical Property of [1,2,4]Triazol-1-yl-phosphonic acid 2-chloro-phenyl ester (2R,3S,5R)-2-[(4-methoxy-phenyl)-diphenyl-methoxymethyl]-5-(5-methyl-2,4-dioxo-3,4-dihydro-2H-pyrimidin-1-yl)-tetrahydro-furan-3-yl ester

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Technology Process of [1,2,4]Triazol-1-yl-phosphonic acid 2-chloro-phenyl ester (2R,3S,5R)-2-[(4-methoxy-phenyl)-diphenyl-methoxymethyl]-5-(5-methyl-2,4-dioxo-3,4-dihydro-2H-pyrimidin-1-yl)-tetrahydro-furan-3-yl ester

There total 1 articles about [1,2,4]Triazol-1-yl-phosphonic acid 2-chloro-phenyl ester (2R,3S,5R)-2-[(4-methoxy-phenyl)-diphenyl-methoxymethyl]-5-(5-methyl-2,4-dioxo-3,4-dihydro-2H-pyrimidin-1-yl)-tetrahydro-furan-3-yl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 15074-54-1
2-chlorophenyl dichlorophosphate

: 82892-62-4
[1,2,4]Triazol-1-yl-phosphonic acid 2-chloro-phenyl ester (2R,3S,5R)-2-[(4-methoxy-phenyl)-diphenyl-methoxymethyl]-5-(5-methyl-2,4-dioxo-3,4-dihydro-2H-pyrimidin-1-yl)-tetrahydro-furan-3-yl ester

Guidance literature:: Multi-step reaction with 2 steps

1: pyridine / 2 h / Ambient temperature

2: pyridine / 1.5 h / Ambient temperature

With pyridine; In pyridine;
DOI:10.1002/hlca.19810640547

Reference yield:

: 82892-62-4
[1,2,4]Triazol-1-yl-phosphonic acid 2-chloro-phenyl ester (2R,3S,5R)-2-[(4-methoxy-phenyl)-diphenyl-methoxymethyl]-5-(5-methyl-2,4-dioxo-3,4-dihydro-2H-pyrimidin-1-yl)-tetrahydro-furan-3-yl ester

: 82892-78-2
C₅₉H₅₅Cl₂N₅O₁₇P₂

Guidance literature:: Multi-step reaction with 3 steps

1: water

2: 80 percent / TPS-NT

3: triethylamine

With water; 1-(2,4,6-triisopropylbenzenesulfonyl)-3-nitro-1,2,4-triazole; triethylamine;
DOI:10.1021/ja00385a026

Reference yield:

: 82892-62-4
[1,2,4]Triazol-1-yl-phosphonic acid 2-chloro-phenyl ester (2R,3S,5R)-2-[(4-methoxy-phenyl)-diphenyl-methoxymethyl]-5-(5-methyl-2,4-dioxo-3,4-dihydro-2H-pyrimidin-1-yl)-tetrahydro-furan-3-yl ester

: 82892-75-9
C₆₂H₅₈Cl₂N₆O₁₇P₂

Guidance literature:: Multi-step reaction with 2 steps

1: water

2: 80 percent / TPS-NT

With water; 1-(2,4,6-triisopropylbenzenesulfonyl)-3-nitro-1,2,4-triazole;
DOI:10.1021/ja00385a026