4-thia-androsten-3,17-diol 17-benzoate

Base Information

• Chemical Name: 4-thia-androsten-3,17-diol 17-benzoate
• CAS No.: 87126-24-7
• Molecular Formula: C₂₅H₃₂O₃S
• Molecular Weight: 412.593
• Mol file: 87126-24-7.mol

Synonyms:

Chemical Property of 4-thia-androsten-3,17-diol 17-benzoate

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 4-thia-androsten-3,17-diol 17-benzoate

There total 2 articles about 4-thia-androsten-3,17-diol 17-benzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

17β-benzoyloxy-4-thia-5-androsten-3-one (85198-46-5) → 4-thia-androsten-3,17-diol 17-benzoate (87126-24-7)

Guidance literature:

With sodium tetrahydroborate; In tetrahydrofuran; for 0.166667h; Ambient temperature;

DOI:10.1135/cccc19831489

Reference yield:

17β-benzoyloxy-5-oxo-3,5-seco-A-nor-androstan-3-oic acid (10520-95-3) → 4-thia-androsten-3,17-diol 17-benzoate (87126-24-7)

Guidance literature:

Multi-step reaction with 2 steps

1: 210 mg / P₂S₅ / pyridine

2: 105 mg / NaBH₄ / tetrahydrofuran / 0.17 h / Ambient temperature

With sodium tetrahydroborate; tetraphosphorus decasulfide; In tetrahydrofuran; pyridine;

DOI:10.1135/cccc19831489

upstream raw materials:

17β-benzoyloxy-4-thia-5-androsten-3-one

17β-benzoyloxy-5-oxo-3,5-seco-A-nor-androstan-3-oic acid

Refernces